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Residual dipolar couplings by off-magic-angle spinning in solid-state nuclear magnetic resonance spectroscopy

Residual dipolar couplings by off-magic-angle spinning in solid-state nuclear magnetic resonance spectroscopy
Residual dipolar couplings by off-magic-angle spinning in solid-state nuclear magnetic resonance spectroscopy
A solid-state NMR analogue of the solution-state residual dipolar coupling effect is demonstrated. A small misset of the spinning axis by less than 0.5 changes the modulation frequency of spin-echoes, allowing the estimation of internuclear dipole-dipole couplings and hence internuclear distances.
nmr, dynamics, rotating solids
0002-7863
10972-10973
Pileio, Giuseppe
13f78e66-0707-4438-b9c9-6dbd3eb7d4e8
Guo, Ying
7f152e2a-4203-4d54-81fa-7888bfe77b11
Pham, Tran N.
83f36ea6-b9ce-4f25-82d3-54ba3d69b726
Griffin, John M.
6dbd9cb3-45da-4e26-ba03-67d7b1c332d7
Levitt, Malcolm H.
bcc5a80a-e5c5-4e0e-9a9a-249d036747c3
Brown, Steven P.
ecbc78d6-023f-41d3-8e84-bd8c7fbfcbfa
Pileio, Giuseppe
13f78e66-0707-4438-b9c9-6dbd3eb7d4e8
Guo, Ying
7f152e2a-4203-4d54-81fa-7888bfe77b11
Pham, Tran N.
83f36ea6-b9ce-4f25-82d3-54ba3d69b726
Griffin, John M.
6dbd9cb3-45da-4e26-ba03-67d7b1c332d7
Levitt, Malcolm H.
bcc5a80a-e5c5-4e0e-9a9a-249d036747c3
Brown, Steven P.
ecbc78d6-023f-41d3-8e84-bd8c7fbfcbfa

Pileio, Giuseppe, Guo, Ying, Pham, Tran N., Griffin, John M., Levitt, Malcolm H. and Brown, Steven P. (2007) Residual dipolar couplings by off-magic-angle spinning in solid-state nuclear magnetic resonance spectroscopy. Journal of the American Chemical Society, 129 (36), 10972-10973. (doi:10.1021/ja0721115).

Record type: Article

Abstract

A solid-state NMR analogue of the solution-state residual dipolar coupling effect is demonstrated. A small misset of the spinning axis by less than 0.5 changes the modulation frequency of spin-echoes, allowing the estimation of internuclear dipole-dipole couplings and hence internuclear distances.

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Published date: 18 August 2007
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Keywords: nmr, dynamics, rotating solids
Organisations: Chemistry
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Identifiers

Local EPrints ID: 146445
URI: http://eprints.soton.ac.uk/id/eprint/146445
DOI: doi:10.1021/ja0721115
ISSN: 0002-7863
PURE UUID: cd910d46-cb13-480d-ba55-b143d63665d4
ORCID for Giuseppe Pileio: ORCID iD orcid.org/0000-0001-9223-3896
ORCID for Malcolm H. Levitt: ORCID iD orcid.org/0000-0001-9878-1180

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Date deposited: 07 Jun 2010 10:15
Last modified: 14 Mar 2024 02:50

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Contributors

Author: Giuseppe Pileio ORCID iD
Author: Ying Guo
Author: Tran N. Pham
Author: John M. Griffin
Author: Malcolm H. Levitt ORCID iD
Author: Steven P. Brown

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