The electrosynthesis of diaryliodonium salts
Peacock, M. J. and Pletcher, D. (2000) The electrosynthesis of diaryliodonium salts. Tetrahedron Letters, 41, (46), 8995-8998. (doi:10.1016/S0040-4039(00)01620-8).
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Original Publication URL: http://dx.doi.org/10.1016/S0040-4039(00)01620-8
Description/Abstract
A simple, one-step procedure for the synthesis of diaryliodonium salts is described. It is shown that the electrochemical oxidation of an aryl iodide at a carbon felt anode in acetic acid/25% acetic anhydride/5% sulfuric acid in the presence of an arene leads to a diaryliodonium salt in good yield. The method allows the preparation of unsymmetrical, as well as symmetrical diaryliodonium salts.
| Item Type: | Article |
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| Related URLs: | |
| Keywords: | iodine compounds |
| Subjects: | Q Science Q Science > QD Chemistry |
| Divisions: | University Structure - Pre August 2011 > School of Chemistry |
| Item ID: | 19029 |
| Date Deposited: | 15 Dec 2005 |
| Last Modified: | 01 Jun 2011 08:32 |
| Contributors: | Peacock, M. J. (Author) Pletcher, D. (Author) |
| Date: | 11 November 2000 |
| Status: | Published |
| URI: | http://eprints.soton.ac.uk/id/eprint/19029 |
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