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2,4-dihydroxy-1,3-bis(methoxycarbonylmethoxy)calix 4 arene and 1,3-bis(ethoxycarbonylmethoxy)-2,4-dihydroxycalix 4 arene chloroform solvate

2,4-dihydroxy-1,3-bis(methoxycarbonylmethoxy)calix 4 arene and 1,3-bis(ethoxycarbonylmethoxy)-2,4-dihydroxycalix 4 arene chloroform solvate
2,4-dihydroxy-1,3-bis(methoxycarbonylmethoxy)calix 4 arene and 1,3-bis(ethoxycarbonylmethoxy)-2,4-dihydroxycalix 4 arene chloroform solvate
The two title calix[4]arene compounds, C34H32O8, (I), and C36H36O8.CH3Cl, (II), respectively, which differ only in the size of the alkyl function on the pendant ester group, are compared. Compound (I) forms a novel supramolecular array, whilst (II) fails to do so due to accommodating a chloroform guest molecule in the lower-rim cavity.
O29-O31
Coles, S. J.
3116f58b-c30c-48cf-bdd5-397d1c1fecf8
Hall, C. W.
6594f171-9eac-4576-8226-8a2a86a62f79
Hursthouse, M. B.
57a2ddf9-b1b3-4f38-bfe9-ef2f526388da
Coles, S. J.
3116f58b-c30c-48cf-bdd5-397d1c1fecf8
Hall, C. W.
6594f171-9eac-4576-8226-8a2a86a62f79
Hursthouse, M. B.
57a2ddf9-b1b3-4f38-bfe9-ef2f526388da

Coles, S. J., Hall, C. W. and Hursthouse, M. B. (2002) 2,4-dihydroxy-1,3-bis(methoxycarbonylmethoxy)calix 4 arene and 1,3-bis(ethoxycarbonylmethoxy)-2,4-dihydroxycalix 4 arene chloroform solvate. Acta Crystallographica Section C: Crystal Structure Communications, 58 (1), O29-O31. (doi:10.1107/S0108270101019163).

Record type: Article

Abstract

The two title calix[4]arene compounds, C34H32O8, (I), and C36H36O8.CH3Cl, (II), respectively, which differ only in the size of the alkyl function on the pendant ester group, are compared. Compound (I) forms a novel supramolecular array, whilst (II) fails to do so due to accommodating a chloroform guest molecule in the lower-rim cavity.

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Published date: 1 January 2002
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Identifiers

Local EPrints ID: 19702
URI: http://eprints.soton.ac.uk/id/eprint/19702
DOI: doi:10.1107/S0108270101019163
PURE UUID: 4a978cb2-544d-46b4-aa23-48c6a216239a
ORCID for S. J. Coles: ORCID iD orcid.org/0000-0001-8414-9272

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Date deposited: 16 Feb 2006
Last modified: 16 Mar 2024 03:05

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Contributors

Author: S. J. Coles ORCID iD
Author: C. W. Hall
Author: M. B. Hursthouse

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