Synthesis of functionalized 1,5-cyclooctadienes by LICKOR metalation

Revell, J. D. and Ganesan, A. (2002) Synthesis of functionalized 1,5-cyclooctadienes by LICKOR metalation. Journal of Organic Chemistry, 67, (17), 6250-6252. (doi:10.1021/jo025715u).


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1,5-Cyclooctadiene was lithiated under LICKOR superbase conditions followed by reaction with alkyl halides or ethylene oxide to yield 3-substituted 1,5-cyclooetadienes in high yield and purity. This procedure is suitable for preparation of 1,5-cyclooctadienes carrying pendant functional groups for immobilization on solid-phase resins.

Item Type: Article
Digital Object Identifier (DOI): doi:10.1021/jo025715u
Related URLs:
Keywords: 9-borabicyclononane 9-bbn, organic-synthesis, superbases, route
Subjects: Q Science
Q Science > QD Chemistry
Divisions : University Structure - Pre August 2011 > School of Chemistry
ePrint ID: 19843
Accepted Date and Publication Date:
23 August 2002Published
Date Deposited: 20 Feb 2006
Last Modified: 31 Mar 2016 11:37

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