Extended X-ray absorption fine structure (EXAFS) characterisation of dilute palladium homogeneous catalysts


Fiddy, S. G., Evans, J., Newton, M. A., Neisius, T., Tooze, R. P. and Oldman, R. (2003) Extended X-ray absorption fine structure (EXAFS) characterisation of dilute palladium homogeneous catalysts. Chemical Communications, (21), 2682-2683. (doi: 10.1039/b307535d).

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Description/Abstract

Highly dilute EXAFS characterisation for the elucidation of species involved in Heck chemistry is demonstrated; the major "monomer" species of Herrmann's acetate-bridged phosphapalladadacycle is characterised and species present during the course of a 50 ppm [Pd] Pd(OAc)(2)/PBu3t catalysed Heck reaction are presented.

Item Type: Article
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Keywords: aryl chlorides, bromides, acetate, mild
Subjects: Q Science
Q Science > QD Chemistry
Divisions: University Structure - Pre August 2011 > School of Chemistry
ePrint ID: 19950
Date Deposited: 21 Feb 2006
Last Modified: 27 Mar 2014 18:09
URI: http://eprints.soton.ac.uk/id/eprint/19950

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