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Decarboxylation of fluorosulfones for the preparation fluoroalkylidene precursors

Decarboxylation of fluorosulfones for the preparation fluoroalkylidene precursors
Decarboxylation of fluorosulfones for the preparation fluoroalkylidene precursors
The synthesis of fluorosulfones by alkylation of fluoroacetate derivatives is reported. Their decarboxylation reaction under Krapcho conditions is a convenient process to prepare fluorosulfones as reagents for fluoroalkene synthesis.
fluorosulfones, benzothiazole, julia–kocienski reaction, krapcho, decarboxylation
0022-1139
128-135
Larnaud, Florent
b5b03dcb-6c7e-4232-8a38-4bf904805a18
Pfund, Emmanuel
ecfd6437-1953-4e22-9638-42d0d9f11bed
Linclau, Bruno
19b9cacd-b8e8-4c65-af36-6352cade84ba
Lequeux, Thierry
52eca0ba-760f-457b-9d61-52df125721b2
Larnaud, Florent
b5b03dcb-6c7e-4232-8a38-4bf904805a18
Pfund, Emmanuel
ecfd6437-1953-4e22-9638-42d0d9f11bed
Linclau, Bruno
19b9cacd-b8e8-4c65-af36-6352cade84ba
Lequeux, Thierry
52eca0ba-760f-457b-9d61-52df125721b2

Larnaud, Florent, Pfund, Emmanuel, Linclau, Bruno and Lequeux, Thierry (2012) Decarboxylation of fluorosulfones for the preparation fluoroalkylidene precursors. [in special issue: Fluorine Chemistry in France] Journal of Fluorine Chemistry, 134, 128-135. (doi:10.1016/j.jfluchem.2011.03.005).

Record type: Article

Abstract

The synthesis of fluorosulfones by alkylation of fluoroacetate derivatives is reported. Their decarboxylation reaction under Krapcho conditions is a convenient process to prepare fluorosulfones as reagents for fluoroalkene synthesis.

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More information

e-pub ahead of print date: 15 March 2011
Published date: February 2012
Keywords: fluorosulfones, benzothiazole, julia–kocienski reaction, krapcho, decarboxylation
Organisations: Chemistry
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Identifiers

Local EPrints ID: 208717
URI: http://eprints.soton.ac.uk/id/eprint/208717
DOI: doi:10.1016/j.jfluchem.2011.03.005
ISSN: 0022-1139
PURE UUID: 899ccca7-0f5d-44ab-8c53-7cd2636ae6b7
ORCID for Bruno Linclau: ORCID iD orcid.org/0000-0001-8762-0170

Catalogue record

Date deposited: 23 Jan 2012 11:06
Last modified: 15 Mar 2024 03:05

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Contributors

Author: Florent Larnaud
Author: Emmanuel Pfund
Author: Bruno Linclau ORCID iD
Author: Thierry Lequeux

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