Design and performance of a microsecond time-resolved photo-chemically induced dynamic nuclear polarization add-on for a high-field nuclear magnetic resonance spectrometer
Design and performance of a microsecond time-resolved photo-chemically induced dynamic nuclear polarization add-on for a high-field nuclear magnetic resonance spectrometer
We describe the design and operation of microsecond time-resolved photo-chemically induced dynamic nuclear polarization hardware, designed to go with a commercial 600 MHz nuclear magnetic resonance (NMR) spectrometer. A frequency-tripled neodymium-doped yttrium/aluminum garnet (Nd:YAG) laser is used as the light source, with a system of mirrors or prisms to route light to the NMR sample from above, removing the need for NMR probe modifications. The experiment has been designed for a shared NMR spectrometer and is straightforward and inexpensive to assemble and operate.
084103-[7pp]
Kuprov, I.
bb07f28a-5038-4524-8146-e3fc8344c065
Goez, M.
6bd02659-c5b1-4cde-868e-86fdfc490dde
Abbott, P.A.
97a60377-324c-419e-9089-bf4c93958332
Hore, P.J.
cad4561e-9571-4b49-b633-1c0bb470d144
2005
Kuprov, I.
bb07f28a-5038-4524-8146-e3fc8344c065
Goez, M.
6bd02659-c5b1-4cde-868e-86fdfc490dde
Abbott, P.A.
97a60377-324c-419e-9089-bf4c93958332
Hore, P.J.
cad4561e-9571-4b49-b633-1c0bb470d144
Kuprov, I., Goez, M., Abbott, P.A. and Hore, P.J.
(2005)
Design and performance of a microsecond time-resolved photo-chemically induced dynamic nuclear polarization add-on for a high-field nuclear magnetic resonance spectrometer.
Review of Scientific Instruments, 76 (8), .
(doi:10.1063/1.2010287).
Abstract
We describe the design and operation of microsecond time-resolved photo-chemically induced dynamic nuclear polarization hardware, designed to go with a commercial 600 MHz nuclear magnetic resonance (NMR) spectrometer. A frequency-tripled neodymium-doped yttrium/aluminum garnet (Nd:YAG) laser is used as the light source, with a system of mirrors or prisms to route light to the NMR sample from above, removing the need for NMR probe modifications. The experiment has been designed for a shared NMR spectrometer and is straightforward and inexpensive to assemble and operate.
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e-pub ahead of print date: 15 August 2005
Published date: 2005
Organisations:
Computational Systems Chemistry
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Local EPrints ID: 347393
URI: http://eprints.soton.ac.uk/id/eprint/347393
ISSN: 0034-6748
PURE UUID: 3a50ccad-0e71-46d8-b65a-9ebd5a0f5c9c
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Date deposited: 27 Feb 2013 12:24
Last modified: 15 Mar 2024 03:43
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Author:
M. Goez
Author:
P.A. Abbott
Author:
P.J. Hore
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