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A practical synthesis of a high-loading solid-supported IBX amide for the oxidation of alcohols

A practical synthesis of a high-loading solid-supported IBX amide for the oxidation of alcohols
A practical synthesis of a high-loading solid-supported IBX amide for the oxidation of alcohols
A straightforward three-step synthesis of a solid-supported IBX amide resin was achieved using inexpensive and commercially available 2-iodobenzoic acid chloride and Merrifield resin. A high apparent loading of 0.63 mmol g?1 was obtained. Oxidation of a range of alcohols to the corresponding carbonyl compounds proved very straightforward using 1.2 equiv of the resin. Recycling of the resin was also possible with minimal loss of activity after two reoxidations.
341-351
Lecarpentier, Patrick
cc040af5-614c-45e9-bc64-8b14cde34e8e
Crosignani, Stefano
aaa5cc3f-0b82-4d33-af01-59115c8bdff5
Linclau, Bruno
19b9cacd-b8e8-4c65-af36-6352cade84ba
Lecarpentier, Patrick
cc040af5-614c-45e9-bc64-8b14cde34e8e
Crosignani, Stefano
aaa5cc3f-0b82-4d33-af01-59115c8bdff5
Linclau, Bruno
19b9cacd-b8e8-4c65-af36-6352cade84ba

Lecarpentier, Patrick, Crosignani, Stefano and Linclau, Bruno (2005) A practical synthesis of a high-loading solid-supported IBX amide for the oxidation of alcohols. Molecular Diversity, 9 (4), 341-351. (doi:10.1007/s11030-005-8105-2).

Record type: Article

Abstract

A straightforward three-step synthesis of a solid-supported IBX amide resin was achieved using inexpensive and commercially available 2-iodobenzoic acid chloride and Merrifield resin. A high apparent loading of 0.63 mmol g?1 was obtained. Oxidation of a range of alcohols to the corresponding carbonyl compounds proved very straightforward using 1.2 equiv of the resin. Recycling of the resin was also possible with minimal loss of activity after two reoxidations.

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Published date: 2005
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Identifiers

Local EPrints ID: 37576
URI: http://eprints.soton.ac.uk/id/eprint/37576
DOI: doi:10.1007/s11030-005-8105-2
PURE UUID: 48f32a33-e555-4745-8320-4c2702b9b1c0
ORCID for Bruno Linclau: ORCID iD orcid.org/0000-0001-8762-0170

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Date deposited: 24 May 2006
Last modified: 16 Mar 2024 03:15

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Contributors

Author: Patrick Lecarpentier
Author: Stefano Crosignani
Author: Bruno Linclau ORCID iD

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