Microwave-accelerated O-alkylation of carboxylic acids with O-alkylisoureas
Crosignani, Stefano, White, Peter D and Linclau, Bruno (2002) Microwave-accelerated O-alkylation of carboxylic acids with O-alkylisoureas. Organic letters, 4, (17), 2961-2963. (doi:10.1021/ol0263705).
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Description/Abstract
Microwave-assisted O-alkylations of several carboxylic acids have been performed with three different O-alkylisoureas. All reactions are significantly faster compared to conventionally heated reactions, while retaining high chemoselectivity. The combination of microwave technology with the use of the solid-supported isourea 3 enables the synthetic chemist to obtain the pure methyl esters starting from the corresponding acids in less than an hour.
| Item Type: | Article |
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| Related URLs: | |
| Subjects: | Q Science > QD Chemistry |
| Divisions: | University Structure - Pre August 2011 > School of Chemistry |
| Item ID: | 37589 |
| Date Deposited: | 24 May 2006 |
| Last Modified: | 12 Jul 2012 09:12 |
| Contributors: | Crosignani, Stefano (Author) White, Peter D (Author) Linclau, Bruno (Author) |
| Date: | 2002 |
| Status: | Published |
| Contact Email Address: | bruno.linclau@soton.ac.uk |
| URI: | http://eprints.soton.ac.uk/id/eprint/37589 |
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