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Effect of temperature on microstructural stabilization and mechanical properties in the dynamic testing of nanocrystalline pure Ti

Effect of temperature on microstructural stabilization and mechanical properties in the dynamic testing of nanocrystalline pure Ti
Effect of temperature on microstructural stabilization and mechanical properties in the dynamic testing of nanocrystalline pure Ti
Commercial purity (CP) Ti was processed by a two-step procedure of ECAP and drawing to give a nanocrystalline (NC) grain size of ~90 nm. Samples were tested in compression at a strain rate of 10 s?1 over the temperature range of 298?673 K. The results show the high stored energy and high interface energy promote the process of static recrystallization (SRX) when the NC Ti is heated above 573 K. Migration dynamic recrystallization (m-DRX) operates during compressive deformation at temperatures of 298?573 K giving a homogeneous microstructure. The compressive yield strength and peak stress at 298 K were measured as 1230 and 1330 MPa, respectively. When the test temperature is increased from 298 to 673 K, the yield strength and peak stress decrease and the work hardening rate and dynamic softening rate are also reduced.
drawing, dynamic testing, equal-channel angular pressing, microstructure, titanium
0921-5093
64-70
Zhang, Shixiong
48cab2f9-3e6f-4065-9b8b-bdfeb9b10468
Wang, Ying Chun
5c067a6f-de5d-4fcb-9b0d-80a42c3634b0
Zhilyaev, Alexander P.
d053e518-1976-4633-8953-e8f34b9b7c44
Gunderov, Dmitry V.
b2fef524-a3d4-4fec-b0ca-4293482a3115
Li, Shukui
cf36cc37-f03a-4b4c-8f34-590354846838
Raab, Georgy I.
7561dd79-c69c-42bd-828a-bfc1a42a776f
Korznikova, Elena
6a623244-e24f-4b73-8ae6-e569be301dd1
Langdon, Terence G.
86e69b4f-e16d-4830-bf8a-5a9c11f0de86
Zhang, Shixiong
48cab2f9-3e6f-4065-9b8b-bdfeb9b10468
Wang, Ying Chun
5c067a6f-de5d-4fcb-9b0d-80a42c3634b0
Zhilyaev, Alexander P.
d053e518-1976-4633-8953-e8f34b9b7c44
Gunderov, Dmitry V.
b2fef524-a3d4-4fec-b0ca-4293482a3115
Li, Shukui
cf36cc37-f03a-4b4c-8f34-590354846838
Raab, Georgy I.
7561dd79-c69c-42bd-828a-bfc1a42a776f
Korznikova, Elena
6a623244-e24f-4b73-8ae6-e569be301dd1
Langdon, Terence G.
86e69b4f-e16d-4830-bf8a-5a9c11f0de86

Zhang, Shixiong, Wang, Ying Chun, Zhilyaev, Alexander P., Gunderov, Dmitry V., Li, Shukui, Raab, Georgy I., Korznikova, Elena and Langdon, Terence G. (2015) Effect of temperature on microstructural stabilization and mechanical properties in the dynamic testing of nanocrystalline pure Ti. Materials Science and Engineering: A, 634, 64-70. (doi:10.1016/j.msea.2015.03.032).

Record type: Article

Abstract

Commercial purity (CP) Ti was processed by a two-step procedure of ECAP and drawing to give a nanocrystalline (NC) grain size of ~90 nm. Samples were tested in compression at a strain rate of 10 s?1 over the temperature range of 298?673 K. The results show the high stored energy and high interface energy promote the process of static recrystallization (SRX) when the NC Ti is heated above 573 K. Migration dynamic recrystallization (m-DRX) operates during compressive deformation at temperatures of 298?573 K giving a homogeneous microstructure. The compressive yield strength and peak stress at 298 K were measured as 1230 and 1330 MPa, respectively. When the test temperature is increased from 298 to 673 K, the yield strength and peak stress decrease and the work hardening rate and dynamic softening rate are also reduced.

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More information

Accepted/In Press date: 6 March 2015
e-pub ahead of print date: 18 March 2015
Published date: 14 May 2015
Keywords: drawing, dynamic testing, equal-channel angular pressing, microstructure, titanium
Organisations: Engineering Mats & Surface Engineerg Gp

Identifiers

Local EPrints ID: 377252
URI: http://eprints.soton.ac.uk/id/eprint/377252
ISSN: 0921-5093
PURE UUID: f665b78a-bf89-4cd7-a2ba-813f1907f0b5
ORCID for Terence G. Langdon: ORCID iD orcid.org/0000-0003-3541-9250

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Date deposited: 20 May 2015 14:07
Last modified: 15 Mar 2024 03:13

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Contributors

Author: Shixiong Zhang
Author: Ying Chun Wang
Author: Alexander P. Zhilyaev
Author: Dmitry V. Gunderov
Author: Shukui Li
Author: Georgy I. Raab
Author: Elena Korznikova

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