Trans-dibromodioxodimethylformamide molybdenum(VI) MoO2Br2(OCHNMe2)(2)
Drake, J.E., Hursthouse, M.B., Light, M.E., Kumar, R. and Ratnani, R. (2007) Trans-dibromodioxodimethylformamide molybdenum(VI) MoO2Br2(OCHNMe2)(2). Journal of Chemical Crystallography, 37, (6), 421-427. (doi:10.1007/s10870-007-9186-9).
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Description/Abstract
The molecular structure of Trans-dibromodioxodimethylformamide molybdenum(VI), MoO2Br2(OCHNMe2)2 has been determined. Crystal data: Triclinic, P-1, a = 12.3005(2), b = 15.8763(4), c = 21.1653(6) Å, α = 71.992(1)°, β = 88.966(2)°, γ = 89.999(1)°, V = 3930.1(2) Å, Z = 12. Trans-dibromodioxodimethylformamide molybdenum(VI) was obtained by the reaction of sodium molybdate, HBr and dimethylformamide and was characterized by IR, and 1H NMR spectroscopy and elemental analysis.
| Item Type: | Article |
|---|---|
| ISSNs: | 1074-1542 (print) |
| Related URLs: | |
| Keywords: | spectroscopic characterization, complexes, nmr, dimethylformamide, crystal-structures, molybdenum, ethers, x-ray analysis, synthesis, molecular-structure, addition-compounds |
| Subjects: | Q Science > QD Chemistry |
| Divisions: | University Structure - Pre August 2011 > School of Chemistry |
| Item ID: | 54286 |
| Date Deposited: | 31 Jul 2008 |
| Last Modified: | 01 Jun 2011 09:29 |
| Contributors: | Drake, J.E. (Author) Hursthouse, M.B. (Author) Light, M.E. (Author) Kumar, R. (Author) Ratnani, R. (Author) |
| Date: | 2007 |
| Status: | Published |
| URI: | http://eprints.soton.ac.uk/id/eprint/54286 |
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