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4,4,6,6-tetrachloro-2-[(2,4-dimethylphenyl)sulfanyl]-N-[4-(2,2,4,4-tetra chloro-1,3,5,7,11-pentaaza-2 lambda(5),4 lambda(5),6 lambda(5)-triphosphaspiro[5.5] undeca-1,3,5-trien7-yl)butyl]-1,3,5,2 lambda(5),4 lambda(5),6 lambda(5)-triaza-triphosphinin-2-amine

4,4,6,6-tetrachloro-2-[(2,4-dimethylphenyl)sulfanyl]-N-[4-(2,2,4,4-tetra chloro-1,3,5,7,11-pentaaza-2 lambda(5),4 lambda(5),6 lambda(5)-triphosphaspiro[5.5] undeca-1,3,5-trien7-yl)butyl]-1,3,5,2 lambda(5),4 lambda(5),6 lambda(5)-triaza-triphosphinin-2-amine
4,4,6,6-tetrachloro-2-[(2,4-dimethylphenyl)sulfanyl]-N-[4-(2,2,4,4-tetra chloro-1,3,5,7,11-pentaaza-2 lambda(5),4 lambda(5),6 lambda(5)-triphosphaspiro[5.5] undeca-1,3,5-trien7-yl)butyl]-1,3,5,2 lambda(5),4 lambda(5),6 lambda(5)-triaza-triphosphinin-2-amine
Reaction of the spermidine-bridged cyclophosphazene compound (N3P3Cl5)spd(N3P3Cl4) (spd = spermidine residue) with 2,4-dimethylthiophenol results in substitution of the P-Cl bond at the bridgehead >P(NHR)Cl group to give the title compound, C15H25Cl8N9P6S. An N-H...N hydrogen bond helps to establish the packing.
O3753-U2529
Coles, S.J.
3116f58b-c30c-48cf-bdd5-397d1c1fecf8
Davies, D.B.
bf1a738f-6739-4e53-ad8b-f860b599f597
Hursthouse, M.B.
57a2ddf9-b1b3-4f38-bfe9-ef2f526388da
Ibisoglu, H.
d02665c2-a86b-4013-b6f9-48902447e2f7
Kilic, A.
1406287f-d0aa-4211-b97a-1853ec5ee5b1
Shaw, R.A.
2b5836d0-91f9-468a-b7fe-365beb0a4052
Coles, S.J.
3116f58b-c30c-48cf-bdd5-397d1c1fecf8
Davies, D.B.
bf1a738f-6739-4e53-ad8b-f860b599f597
Hursthouse, M.B.
57a2ddf9-b1b3-4f38-bfe9-ef2f526388da
Ibisoglu, H.
d02665c2-a86b-4013-b6f9-48902447e2f7
Kilic, A.
1406287f-d0aa-4211-b97a-1853ec5ee5b1
Shaw, R.A.
2b5836d0-91f9-468a-b7fe-365beb0a4052

Coles, S.J., Davies, D.B., Hursthouse, M.B., Ibisoglu, H., Kilic, A. and Shaw, R.A. (2007) 4,4,6,6-tetrachloro-2-[(2,4-dimethylphenyl)sulfanyl]-N-[4-(2,2,4,4-tetra chloro-1,3,5,7,11-pentaaza-2 lambda(5),4 lambda(5),6 lambda(5)-triphosphaspiro[5.5] undeca-1,3,5-trien7-yl)butyl]-1,3,5,2 lambda(5),4 lambda(5),6 lambda(5)-triaza-triphosphinin-2-amine. Acta Crystallographica Section E: Crystallographic Communications, 63 (9), O3753-U2529. (doi:10.1107/S1600536807038962).

Record type: Article

Abstract

Reaction of the spermidine-bridged cyclophosphazene compound (N3P3Cl5)spd(N3P3Cl4) (spd = spermidine residue) with 2,4-dimethylthiophenol results in substitution of the P-Cl bond at the bridgehead >P(NHR)Cl group to give the title compound, C15H25Cl8N9P6S. An N-H...N hydrogen bond helps to establish the packing.

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Published date: 2007
Organisations: Chemistry
Learn more about Chemistry research

Identifiers

Local EPrints ID: 150703
URI: http://eprints.soton.ac.uk/id/eprint/150703
DOI: doi:10.1107/S1600536807038962
PURE UUID: 1a3cb5ec-4fbc-4c00-85c6-bd3748b97bdc
ORCID for S.J. Coles: ORCID iD orcid.org/0000-0001-8414-9272

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Date deposited: 03 Jun 2010 09:20
Last modified: 14 Mar 2024 02:43

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Author: S.J. Coles ORCID iD
Author: D.B. Davies
Author: M.B. Hursthouse
Author: H. Ibisoglu
Author: A. Kilic
Author: R.A. Shaw

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