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Samarium diiodide mediated intramolecular cyclisation of mixed enone-enoate systems: a simple preparation of spirocyclic ethers

Samarium diiodide mediated intramolecular cyclisation of mixed enone-enoate systems: a simple preparation of spirocyclic ethers
Samarium diiodide mediated intramolecular cyclisation of mixed enone-enoate systems: a simple preparation of spirocyclic ethers
Samarium(II) diiodide mediated intramolecular cyclisation of mixed enone–enoate substrates in THF/MeOH is described. Spirocyclic ethers are obtained, and the stereodefined preparation of 1-oxaspiro[4.4]nonan-7-one products is included.

samarium(II) diiodide, reductive cyclisation, michael addition, spirocycle, chelation control
0040-4039
928-931
Meng, Junxiu
4826e3e4-b519-4040-b4ab-98f24358f08a
Light, Mark E.
cf57314e-6856-491b-a8d2-2dffc452e161
Kilburn, Jeremy D.
e64ded70-825a-40ec-816b-c4605e007e7a
Dixon, Sally
943160fc-1b70-4c29-b2e3-b7785cee8a0c
Meng, Junxiu
4826e3e4-b519-4040-b4ab-98f24358f08a
Light, Mark E.
cf57314e-6856-491b-a8d2-2dffc452e161
Kilburn, Jeremy D.
e64ded70-825a-40ec-816b-c4605e007e7a
Dixon, Sally
943160fc-1b70-4c29-b2e3-b7785cee8a0c

Meng, Junxiu, Light, Mark E., Kilburn, Jeremy D. and Dixon, Sally (2011) Samarium diiodide mediated intramolecular cyclisation of mixed enone-enoate systems: a simple preparation of spirocyclic ethers. Tetrahedron Letters, 52 (8), 928-931. (doi:10.1016/j.tetlet.2010.12.077).

Record type: Article

Abstract

Samarium(II) diiodide mediated intramolecular cyclisation of mixed enone–enoate substrates in THF/MeOH is described. Spirocyclic ethers are obtained, and the stereodefined preparation of 1-oxaspiro[4.4]nonan-7-one products is included.

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More information

Published date: 23 February 2011
Keywords: samarium(II) diiodide, reductive cyclisation, michael addition, spirocycle, chelation control
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Identifiers

Local EPrints ID: 176335
URI: http://eprints.soton.ac.uk/id/eprint/176335
DOI: doi:10.1016/j.tetlet.2010.12.077
ISSN: 0040-4039
PURE UUID: 778ca998-512d-46c2-82db-9d594cf40425
ORCID for Mark E. Light: ORCID iD orcid.org/0000-0002-0585-0843
ORCID for Sally Dixon: ORCID iD orcid.org/0000-0003-2219-3635

Catalogue record

Date deposited: 08 Mar 2011 10:16
Last modified: 14 Mar 2024 02:46

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Contributors

Author: Junxiu Meng
Author: Mark E. Light ORCID iD
Author: Jeremy D. Kilburn
Author: Sally Dixon ORCID iD

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