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The synthesis and characterisation of bis(phenylpyridylphosphino)ethane

The synthesis and characterisation of bis(phenylpyridylphosphino)ethane
The synthesis and characterisation of bis(phenylpyridylphosphino)ethane
A novel synthesis has been devised for the preparation of unsymmetrical phosphine substituted derivatives of bis(diphenylphosphino)ethane [dppe]. The title ligand has been prepared in a two step procedure from dppe. A palladium(II) complex of this new ligand has been prepared and characterised by single crystal X-ray diffraction.
pyridine, pyridylphosphines, ligand ray crystal-structures, complex, dippe=1, 2-bis(diisopropylphosphino)ethane, phosphines, 2-pyridyl, chemistry, ligands
0022-328X
103-107
Butler, I. R.
d8a1fc6e-b2be-42fe-b655-c65b803c8903
Licence, P.
725c4e8d-aa44-4663-8fbf-6b6e1f98305e
Coles, S. J.
503a9d9c-0380-4fcd-ad31-cd329255c08e
Hursthouse, M. B.
276e7125-0773-43f6-97e3-77106e9b6e8f
Butler, I. R.
d8a1fc6e-b2be-42fe-b655-c65b803c8903
Licence, P.
725c4e8d-aa44-4663-8fbf-6b6e1f98305e
Coles, S. J.
503a9d9c-0380-4fcd-ad31-cd329255c08e
Hursthouse, M. B.
276e7125-0773-43f6-97e3-77106e9b6e8f

Butler, I. R., Licence, P., Coles, S. J. and Hursthouse, M. B. (2000) The synthesis and characterisation of bis(phenylpyridylphosphino)ethane. Journal of Organometallic Chemistry, 598 (1), 103-107. (doi:10.1016/S0022-328X(99)00683-X).

Record type: Article

Abstract

A novel synthesis has been devised for the preparation of unsymmetrical phosphine substituted derivatives of bis(diphenylphosphino)ethane [dppe]. The title ligand has been prepared in a two step procedure from dppe. A palladium(II) complex of this new ligand has been prepared and characterised by single crystal X-ray diffraction.

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More information

Published date: 25 March 2000
Keywords: pyridine, pyridylphosphines, ligand ray crystal-structures, complex, dippe=1, 2-bis(diisopropylphosphino)ethane, phosphines, 2-pyridyl, chemistry, ligands

Identifiers

Local EPrints ID: 18890
URI: http://eprints.soton.ac.uk/id/eprint/18890
ISSN: 0022-328X
PURE UUID: 0ba61e31-2813-4a40-b01e-7c72eada94ab

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Date deposited: 05 Jan 2006
Last modified: 15 Jul 2019 19:28

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