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A new method of forming resin bound thioesters and their use as ‘traceless’ linkers in solid phase synthesis

Record type: Article

Resin bound thioesters can be prepared by heating thioamides in aqueous DMF with Merrifield resin in the presence of sodium iodide. These thioamides can be cleaved to give alcohols, ketones and lactones by a variety of methods.

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Citation

May, P. J., Bradley, M., Harrowven, D. C. and Pallin, D. (2000) A new method of forming resin bound thioesters and their use as ‘traceless’ linkers in solid phase synthesis Tetrahedron Letters, 41, (10), pp. 1627-1630. (doi:10.1016/S0040-4039(99)02345-X).

More information

Published date: 4 March 2000
Keywords: combinatorial chemistry, lactones, solid phase synthesis, thioamide, thioestersilyl enol ethers, organic-synthesis, esters

Identifiers

Local EPrints ID: 18951
URI: http://eprints.soton.ac.uk/id/eprint/18951
ISSN: 0040-4039
PURE UUID: 15519a27-a8d2-4d0b-9189-94d962cff6ac

Catalogue record

Date deposited: 15 Dec 2005
Last modified: 17 Jul 2017 16:34

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Contributors

Author: P. J. May
Author: M. Bradley
Author: D. C. Harrowven
Author: D. Pallin

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