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Isolation and spectroscopic characterisation of C60F18CF2, the first difluoromethano 60 fullerene

Isolation and spectroscopic characterisation of C60F18CF2, the first difluoromethano 60 fullerene
Isolation and spectroscopic characterisation of C60F18CF2, the first difluoromethano 60 fullerene
From the fluorination of [60]fullerene by K2PtF6 at 465 degrees C under 0.1 bar, we have isolated and characterised C60F18CF2 which has C-s symmetry and is isostructural with C60F18O; it co-elutes (HPLC) with a minor unsymmetrical isomer.
adducts, c-60
1-3
Avent, A. G.
bd34ffe6-fea1-4e75-81fc-82ecaa0c0b5a
Boltalina, O. V.
c91e33b3-7da7-4481-95f4-92fce2a56e46
Lukonin, A. Y.
758144bd-dfdd-42fa-bf14-c73bf69e8f53
Street, J. M.
67b5e419-1784-425f-a913-f67d1fae8b22
Taylor, R.
1abcd415-ae2c-4e95-a761-6948ce7f4d32
Avent, A. G.
bd34ffe6-fea1-4e75-81fc-82ecaa0c0b5a
Boltalina, O. V.
c91e33b3-7da7-4481-95f4-92fce2a56e46
Lukonin, A. Y.
758144bd-dfdd-42fa-bf14-c73bf69e8f53
Street, J. M.
67b5e419-1784-425f-a913-f67d1fae8b22
Taylor, R.
1abcd415-ae2c-4e95-a761-6948ce7f4d32

Avent, A. G., Boltalina, O. V., Lukonin, A. Y., Street, J. M. and Taylor, R. (2000) Isolation and spectroscopic characterisation of C60F18CF2, the first difluoromethano 60 fullerene. Journal of the Chemical Society, Perkin Transactions 2, (1), 1-3. (doi:10.1039/a909157b).

Record type: Article

Abstract

From the fluorination of [60]fullerene by K2PtF6 at 465 degrees C under 0.1 bar, we have isolated and characterised C60F18CF2 which has C-s symmetry and is isostructural with C60F18O; it co-elutes (HPLC) with a minor unsymmetrical isomer.

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More information

Published date: 1 January 2000
Keywords: adducts, c-60

Identifiers

Local EPrints ID: 18989
URI: http://eprints.soton.ac.uk/id/eprint/18989
PURE UUID: c1c0cb79-0957-4c05-a842-6911343772ad

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Date deposited: 21 Dec 2005
Last modified: 15 Mar 2024 06:09

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Contributors

Author: A. G. Avent
Author: O. V. Boltalina
Author: A. Y. Lukonin
Author: J. M. Street
Author: R. Taylor

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