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The electrosynthesis of diaryliodonium salts

Record type: Article

A simple, one-step procedure for the synthesis of diaryliodonium salts is described. It is shown that the electrochemical oxidation of an aryl iodide at a carbon felt anode in acetic acid/25% acetic anhydride/5% sulfuric acid in the presence of an arene leads to a diaryliodonium salt in good yield. The method allows the preparation of unsymmetrical, as well as symmetrical diaryliodonium salts.

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Citation

Peacock, M. J. and Pletcher, D. (2000) The electrosynthesis of diaryliodonium salts Tetrahedron Letters, 41, (46), pp. 8995-8998. (doi:10.1016/S0040-4039(00)01620-8).

More information

Published date: 11 November 2000
Keywords: iodine compounds

Identifiers

Local EPrints ID: 19029
URI: http://eprints.soton.ac.uk/id/eprint/19029
ISSN: 0040-4039
PURE UUID: 17f1e691-4570-4968-9772-7cde68690234

Catalogue record

Date deposited: 15 Dec 2005
Last modified: 17 Jul 2017 16:34

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Contributors

Author: M. J. Peacock
Author: D. Pletcher

University divisions

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