Synthesis and properties of the first series of mixed thioether/telluroether macrocycles
Synthesis and properties of the first series of mixed thioether/telluroether macrocycles
The preparations of the first examples of mixed thioether/telluroether macrocycles, [9]aneS(2)Te (1,4-dithia-7-telluracyclononane), [11]aneS(2)Te (1,4-dithia-8-telluracycloundecane), [12]aneS(2)Te (1,5-dithia-9-telluracyclododecane) and [14]aneS(3)Te (1,4,7-trithia-11-telluracyclotetradecane) via a 'disguised dilution' method are described, together with the crystal structure of [Ag([11]aneS(2)Te)]BF4 which serves to authenticate the macrocyclic ligand.
ditelluroether complexes, crystal-structures, ligands
427-428
Levason, W.
e7f6d7c7-643c-49f5-8b57-0ebbe1bb52cd
Orchard, S. D.
90cbc344-8d53-406f-acf4-ad93cef1ddae
Reid, G.
37d35b11-40ce-48c5-a68e-f6ce04cd4037
2001
Levason, W.
e7f6d7c7-643c-49f5-8b57-0ebbe1bb52cd
Orchard, S. D.
90cbc344-8d53-406f-acf4-ad93cef1ddae
Reid, G.
37d35b11-40ce-48c5-a68e-f6ce04cd4037
Levason, W., Orchard, S. D. and Reid, G.
(2001)
Synthesis and properties of the first series of mixed thioether/telluroether macrocycles.
Chemical Communications, (5), .
(doi:10.1039/b008370o).
Abstract
The preparations of the first examples of mixed thioether/telluroether macrocycles, [9]aneS(2)Te (1,4-dithia-7-telluracyclononane), [11]aneS(2)Te (1,4-dithia-8-telluracycloundecane), [12]aneS(2)Te (1,5-dithia-9-telluracyclododecane) and [14]aneS(3)Te (1,4,7-trithia-11-telluracyclotetradecane) via a 'disguised dilution' method are described, together with the crystal structure of [Ag([11]aneS(2)Te)]BF4 which serves to authenticate the macrocyclic ligand.
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Published date: 2001
Keywords:
ditelluroether complexes, crystal-structures, ligands
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Local EPrints ID: 19547
URI: http://eprints.soton.ac.uk/id/eprint/19547
ISSN: 1359-7345
PURE UUID: 490f25e4-128b-4053-b59e-06fe049b95ce
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Date deposited: 14 Feb 2006
Last modified: 16 Mar 2024 02:43
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Author:
S. D. Orchard
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