(1S*,4S*,5R*,8R*)-8-(3,4-Dimethoxyphenyl)-4-(3,4,5-trimethoxyphenyl)-3,7 -dioxabicyclo 3.3.0 octan-2-one
(1S*,4S*,5R*,8R*)-8-(3,4-Dimethoxyphenyl)-4-(3,4,5-trimethoxyphenyl)-3,7 -dioxabicyclo 3.3.0 octan-2-one
The X-ray study of the title compound, C23H26O8, (I), confirmed the endo,exo-furofuranone structure of the important intermediate compound in the process of the total synthesis of (+/-)-epimagnolin A, which employs a new approach involving a highly diastereoselective CDH insertion reaction [Brown et al. (2001). Tetrahedron Lett. 42, 473-475].
o514-o515
Light, M. E.
cf57314e-6856-491b-a8d2-2dffc452e161
Hursthouse, M. B.
57a2ddf9-b1b3-4f38-bfe9-ef2f526388da
1 June 2001
Light, M. E.
cf57314e-6856-491b-a8d2-2dffc452e161
Hursthouse, M. B.
57a2ddf9-b1b3-4f38-bfe9-ef2f526388da
Light, M. E. and Hursthouse, M. B.
(2001)
(1S*,4S*,5R*,8R*)-8-(3,4-Dimethoxyphenyl)-4-(3,4,5-trimethoxyphenyl)-3,7 -dioxabicyclo 3.3.0 octan-2-one.
Acta Crystallographica Section E: Structure Reports Online, 57 (6), .
(doi:10.1107/S1600536801007425).
Abstract
The X-ray study of the title compound, C23H26O8, (I), confirmed the endo,exo-furofuranone structure of the important intermediate compound in the process of the total synthesis of (+/-)-epimagnolin A, which employs a new approach involving a highly diastereoselective CDH insertion reaction [Brown et al. (2001). Tetrahedron Lett. 42, 473-475].
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Published date: 1 June 2001
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Local EPrints ID: 19557
URI: http://eprints.soton.ac.uk/id/eprint/19557
PURE UUID: 64e2ecfd-1690-46c4-89fe-da3bd732ec21
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Date deposited: 15 Feb 2006
Last modified: 16 Mar 2024 03:04
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