Light, M. E. and Hursthouse, M. B.
(1S*,4S*,5R*,8R*)-8-(3,4-Dimethoxyphenyl)-4-(3,4,5-trimethoxyphenyl)-3,7 -dioxabicyclo 3.3.0 octan-2-one
Acta Crystallographica Section E: Structure Reports Online, 57, (6), . (doi:10.1107/S1600536801007425).
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The X-ray study of the title compound, C23H26O8, (I), confirmed the endo,exo-furofuranone structure of the important intermediate compound in the process of the total synthesis of (+/-)-epimagnolin A, which employs a new approach involving a highly diastereoselective CDH insertion reaction [Brown et al. (2001). Tetrahedron Lett. 42, 473-475].
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