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4,4-Dimethyl-3,5,8,10-tetraoxatricyclo 5.2.1.0(2,6) decane

4,4-Dimethyl-3,5,8,10-tetraoxatricyclo 5.2.1.0(2,6) decane
4,4-Dimethyl-3,5,8,10-tetraoxatricyclo 5.2.1.0(2,6) decane
The title compound, C8H12O4, is formed as a by-product in the preparation of the protected sugar 2,3-O-isopropylidene--D-ribose under acid-catalysed conditions (H2SO4/acetone) from D-ribose [Fleetwood & Hughes (1999). Carbohydr. Res. 317, 204-209]. The absolute configuration was assigned on the basis of the known D-ribose configuration.
o560-o561
Light, M. E.
cf57314e-6856-491b-a8d2-2dffc452e161
Murphy, P. J.
e361583b-6b55-4418-a536-24f3405273a2
Brown, P. M.
b785f4b3-4544-497a-bc51-11eb525615db
Hursthouse, M. B.
57a2ddf9-b1b3-4f38-bfe9-ef2f526388da
Light, M. E.
cf57314e-6856-491b-a8d2-2dffc452e161
Murphy, P. J.
e361583b-6b55-4418-a536-24f3405273a2
Brown, P. M.
b785f4b3-4544-497a-bc51-11eb525615db
Hursthouse, M. B.
57a2ddf9-b1b3-4f38-bfe9-ef2f526388da

Light, M. E., Murphy, P. J., Brown, P. M. and Hursthouse, M. B. (2002) 4,4-Dimethyl-3,5,8,10-tetraoxatricyclo 5.2.1.0(2,6) decane. Acta Crystallographica Section E: Structure Reports Online, 58 (5), o560-o561. (doi:10.1107/S160053680200661X).

Record type: Article

Abstract

The title compound, C8H12O4, is formed as a by-product in the preparation of the protected sugar 2,3-O-isopropylidene--D-ribose under acid-catalysed conditions (H2SO4/acetone) from D-ribose [Fleetwood & Hughes (1999). Carbohydr. Res. 317, 204-209]. The absolute configuration was assigned on the basis of the known D-ribose configuration.

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Published date: 1 May 2002
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Identifiers

Local EPrints ID: 19806
URI: http://eprints.soton.ac.uk/id/eprint/19806
DOI: doi:10.1107/S160053680200661X
PURE UUID: 7ff7c2f2-948a-4354-b6f3-a86ef35468ea
ORCID for M. E. Light: ORCID iD orcid.org/0000-0002-0585-0843

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Date deposited: 16 Feb 2006
Last modified: 16 Mar 2024 03:04

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Author: M. E. Light ORCID iD
Author: P. J. Murphy
Author: P. M. Brown
Author: M. B. Hursthouse

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