Synthesis of functionalized 1,5-cyclooctadienes by LICKOR metalation


Revell, J. D. and Ganesan, A. (2002) Synthesis of functionalized 1,5-cyclooctadienes by LICKOR metalation Journal of Organic Chemistry, 67, (17), pp. 6250-6252. (doi:10.1021/jo025715u).

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Description/Abstract

1,5-Cyclooctadiene was lithiated under LICKOR superbase conditions followed by reaction with alkyl halides or ethylene oxide to yield 3-substituted 1,5-cyclooetadienes in high yield and purity. This procedure is suitable for preparation of 1,5-cyclooctadienes carrying pendant functional groups for immobilization on solid-phase resins.

Item Type: Article
Digital Object Identifier (DOI): doi:10.1021/jo025715u
ISSNs: 0022-3263 (print)
Related URLs:
Keywords: 9-borabicyclononane 9-bbn, organic-synthesis, superbases, route
Subjects:
ePrint ID: 19843
Date :
Date Event
23 August 2002Published
Date Deposited: 20 Feb 2006
Last Modified: 16 Apr 2017 23:00
Further Information:Google Scholar
URI: http://eprints.soton.ac.uk/id/eprint/19843

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