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Proton spectroscopy in solid state nuclear magnetic resonance with windowed phase modulated Lee-Goldburg decoupling sequences

Proton spectroscopy in solid state nuclear magnetic resonance with windowed phase modulated Lee-Goldburg decoupling sequences
Proton spectroscopy in solid state nuclear magnetic resonance with windowed phase modulated Lee-Goldburg decoupling sequences
We demonstrate here a new windowed multiple pulse sequence for the detection of protons in solid state NMR. Acquisition windows are inserted in the phase modulated Lee–Goldburg scheme (PMLG). This enables one-dimensional acquisition as against two-dimensional in windowless schemes. The pulse scheme, theoretical justifications and experimental spectra of a few samples are presented. In addition two-dimensional proton–proton and carbon–proton correlation experiments are performed with windowed PMLG proton detection.
multiple pulse nmr, angle-spinning nmr, rotating solids, cross-polarization
0009-2614
193-202
Vinogradov, Elena
a2ec7b18-a661-416c-93a3-231acb55dd49
Madhu, P.K.
d3e7accb-343e-4ad0-9ef2-56e505202bbb
Vega, Shimon
58f3b892-fbe8-4037-95fb-7eec2689c877
Vinogradov, Elena
a2ec7b18-a661-416c-93a3-231acb55dd49
Madhu, P.K.
d3e7accb-343e-4ad0-9ef2-56e505202bbb
Vega, Shimon
58f3b892-fbe8-4037-95fb-7eec2689c877

Vinogradov, Elena, Madhu, P.K. and Vega, Shimon (2002) Proton spectroscopy in solid state nuclear magnetic resonance with windowed phase modulated Lee-Goldburg decoupling sequences. Chemical Physics Letters, 354 (3-4), 193-202. (doi:10.1016/S0009-2614(02)00060-X).

Record type: Article

Abstract

We demonstrate here a new windowed multiple pulse sequence for the detection of protons in solid state NMR. Acquisition windows are inserted in the phase modulated Lee–Goldburg scheme (PMLG). This enables one-dimensional acquisition as against two-dimensional in windowless schemes. The pulse scheme, theoretical justifications and experimental spectra of a few samples are presented. In addition two-dimensional proton–proton and carbon–proton correlation experiments are performed with windowed PMLG proton detection.

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More information

Published date: 12 March 2002
Keywords: multiple pulse nmr, angle-spinning nmr, rotating solids, cross-polarization

Identifiers

Local EPrints ID: 19867
URI: http://eprints.soton.ac.uk/id/eprint/19867
ISSN: 0009-2614
PURE UUID: ad7d63a9-26c2-4e63-adbb-713b2d7200b6

Catalogue record

Date deposited: 22 Feb 2006
Last modified: 09 Jan 2022 01:21

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Contributors

Author: Elena Vinogradov
Author: P.K. Madhu
Author: Shimon Vega

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