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Application of cogwheel phase cycling to sideband manipulation experiments in solid-state NMR

Application of cogwheel phase cycling to sideband manipulation experiments in solid-state NMR
Application of cogwheel phase cycling to sideband manipulation experiments in solid-state NMR
Cogwheel phase-cycling schemes are applied to sideband suppression and sideband separation experiments in solid-state NMR. It is shown that cogwheel phase cycles lead to the elimination of most pulse imperfection effects, while using far fewer experimental signal acquisitions than conventional phase-cycling methods.
cogwheel phase cycling, spinning sidebands, toss, pass, angle-spinning nmr, chemical-shift anisotropy, order, separation, spectroscopy, suppression, resolution, spectra, frequencies, pathways
286-293
Ivchenko, Natala
5e94869c-fa70-4fef-b6f2-a1f291da8388
Hughes, Colan E.
5054ad30-ed83-4835-9dde-0fafad016711
Levitt, Malcolm H.
bcc5a80a-e5c5-4e0e-9a9a-249d036747c3
Ivchenko, Natala
5e94869c-fa70-4fef-b6f2-a1f291da8388
Hughes, Colan E.
5054ad30-ed83-4835-9dde-0fafad016711
Levitt, Malcolm H.
bcc5a80a-e5c5-4e0e-9a9a-249d036747c3

Ivchenko, Natala, Hughes, Colan E. and Levitt, Malcolm H. (2003) Application of cogwheel phase cycling to sideband manipulation experiments in solid-state NMR. Journal of Magnetic Resonance, 164 (2), 286-293. (doi:10.1016/S1090-7807(03)00206-4).

Record type: Article

Abstract

Cogwheel phase-cycling schemes are applied to sideband suppression and sideband separation experiments in solid-state NMR. It is shown that cogwheel phase cycles lead to the elimination of most pulse imperfection effects, while using far fewer experimental signal acquisitions than conventional phase-cycling methods.

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More information

Published date: 1 October 2003
Keywords: cogwheel phase cycling, spinning sidebands, toss, pass, angle-spinning nmr, chemical-shift anisotropy, order, separation, spectroscopy, suppression, resolution, spectra, frequencies, pathways

Identifiers

Local EPrints ID: 19987
URI: http://eprints.soton.ac.uk/id/eprint/19987
PURE UUID: 5ade0c49-84fc-4412-9eb9-6bb8d5989fae
ORCID for Malcolm H. Levitt: ORCID iD orcid.org/0000-0001-9878-1180

Catalogue record

Date deposited: 23 Feb 2006
Last modified: 16 Mar 2024 03:18

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Contributors

Author: Natala Ivchenko
Author: Colan E. Hughes

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