Multiplex phase cycling
Multiplex phase cycling
We discuss a new class of phase cycling procedures, in which a set of individual phase-shifted transients are stored separately in the computer and processed afterwards to yield the separated NMR signals from two or more coherence transfer pathways. In the case of two-dimensional double-quantum spectroscopy, this multiplex acquisition procedure allows the acquisition of pure-absorption spectra in only 62.5% of the time needed by previous methods.
phase cycling, coherence transfer pathways, multiplex phase cycles, pure-absorption, phase angle-spinning nmr, mqmas nmr, spectra, spectroscopy, coherence, solids, frequencies, pathways, nuclei, signs
52-58
Ivchenko, Natala
5e94869c-fa70-4fef-b6f2-a1f291da8388
Hughes, Colan E.
5054ad30-ed83-4835-9dde-0fafad016711
Levitt, Malcolm H.
bcc5a80a-e5c5-4e0e-9a9a-249d036747c3
1 January 2003
Ivchenko, Natala
5e94869c-fa70-4fef-b6f2-a1f291da8388
Hughes, Colan E.
5054ad30-ed83-4835-9dde-0fafad016711
Levitt, Malcolm H.
bcc5a80a-e5c5-4e0e-9a9a-249d036747c3
Ivchenko, Natala, Hughes, Colan E. and Levitt, Malcolm H.
(2003)
Multiplex phase cycling.
Journal of Magnetic Resonance, 160 (1), .
(doi:10.1016/S1090-7807(02)00108-8).
Abstract
We discuss a new class of phase cycling procedures, in which a set of individual phase-shifted transients are stored separately in the computer and processed afterwards to yield the separated NMR signals from two or more coherence transfer pathways. In the case of two-dimensional double-quantum spectroscopy, this multiplex acquisition procedure allows the acquisition of pure-absorption spectra in only 62.5% of the time needed by previous methods.
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Published date: 1 January 2003
Keywords:
phase cycling, coherence transfer pathways, multiplex phase cycles, pure-absorption, phase angle-spinning nmr, mqmas nmr, spectra, spectroscopy, coherence, solids, frequencies, pathways, nuclei, signs
Identifiers
Local EPrints ID: 19988
URI: http://eprints.soton.ac.uk/id/eprint/19988
PURE UUID: f6caee27-fe87-454f-9371-a0bc91932fa9
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Date deposited: 24 Feb 2006
Last modified: 16 Mar 2024 03:18
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Contributors
Author:
Natala Ivchenko
Author:
Colan E. Hughes
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