KF-silica as a stationary phase for the chromatographic removal of tin residues from organic compounds
KF-silica as a stationary phase for the chromatographic removal of tin residues from organic compounds
Through the simple expedient of using a mixture of KF and silica as the stationary phase in column chromatography, levels of organotin impurities from tributyltin hydride mediated reductions have been reduced from stoichiometric levels to similar to ~ 30 ppm.
intramolecular radical additions, cyclization reactions, atom-transfer, organotin hydrides, reagent, reductions, chemistry, stannane, halides, deoxygenation
1968-1969
Harrowven, David C.
bddcfab6-dbde-49df-aec2-42abbcf5d10b
Guy, Ian L.
b7d1bed5-2418-43d4-bb05-1db8d1bcc2db
2004
Harrowven, David C.
bddcfab6-dbde-49df-aec2-42abbcf5d10b
Guy, Ian L.
b7d1bed5-2418-43d4-bb05-1db8d1bcc2db
Harrowven, David C. and Guy, Ian L.
(2004)
KF-silica as a stationary phase for the chromatographic removal of tin residues from organic compounds.
Chemical Communications, (17), .
(doi:10.1039/b406041e).
Abstract
Through the simple expedient of using a mixture of KF and silica as the stationary phase in column chromatography, levels of organotin impurities from tributyltin hydride mediated reductions have been reduced from stoichiometric levels to similar to ~ 30 ppm.
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Published date: 2004
Keywords:
intramolecular radical additions, cyclization reactions, atom-transfer, organotin hydrides, reagent, reductions, chemistry, stannane, halides, deoxygenation
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Local EPrints ID: 20218
URI: http://eprints.soton.ac.uk/id/eprint/20218
ISSN: 1359-7345
PURE UUID: 95288186-fe13-4a57-b3b4-1dfe521c9b70
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Date deposited: 20 Feb 2006
Last modified: 16 Mar 2024 02:46
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Author:
Ian L. Guy
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