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Bis(nitrato-?2O,O')(1,4,7,10,13-pentaoxacyclopentadecane)calcium(II)

Bis(nitrato-?2O,O')(1,4,7,10,13-pentaoxacyclopentadecane)calcium(II)
Bis(nitrato-?2O,O')(1,4,7,10,13-pentaoxacyclopentadecane)calcium(II)
The crystal structure of the title compound, [Ca(NO3)2- (C10H20O5)], at 120 K contains discrete molecules with ninecoordinate Ca atoms. There are two molecules in the asymmetric unit, related by a pseudo-inversion centre. The crown bonds through five O atoms [Ca—O = 2.464 (2)–2.567 (2) A ° ] and the nitrates are bidentate [Ca—O = 2.444 (2)–2.588 (2) A ° ]. The structure is a polymorph of a previously reported room-temperature form.
m1015-m1017
Brown, M.D.
785195da-02f2-46c7-b482-d8c8516f09ff
Levason, W.
2388863a-5332-4ce5-8264-572fd8ee7d82
Webster, M.
d49b7fa6-3539-4209-b349-d66c61fb34e2
Brown, M.D.
785195da-02f2-46c7-b482-d8c8516f09ff
Levason, W.
2388863a-5332-4ce5-8264-572fd8ee7d82
Webster, M.
d49b7fa6-3539-4209-b349-d66c61fb34e2

Brown, M.D., Levason, W. and Webster, M. (2005) Bis(nitrato-?2O,O')(1,4,7,10,13-pentaoxacyclopentadecane)calcium(II). Acta Crystallographica Section E Crystallographic Communications, 61 (6), m1015-m1017. (doi:10.1107/S1600536805012973).

Record type: Article

Abstract

The crystal structure of the title compound, [Ca(NO3)2- (C10H20O5)], at 120 K contains discrete molecules with ninecoordinate Ca atoms. There are two molecules in the asymmetric unit, related by a pseudo-inversion centre. The crown bonds through five O atoms [Ca—O = 2.464 (2)–2.567 (2) A ° ] and the nitrates are bidentate [Ca—O = 2.444 (2)–2.588 (2) A ° ]. The structure is a polymorph of a previously reported room-temperature form.

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Published date: 2005
Additional Information: Metal-organic compounds

Identifiers

Local EPrints ID: 20745
URI: https://eprints.soton.ac.uk/id/eprint/20745
PURE UUID: 682d6bd6-4748-4d5b-8b31-432b2388dc63

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Date deposited: 02 Mar 2006
Last modified: 17 Jul 2017 16:28

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