Synthesis of a biphenyl library for studies of hydrogen bonding in the solid state
Synthesis of a biphenyl library for studies of hydrogen bonding in the solid state
A biphenyl library incorporating amide and sulfonamide groups has been synthesised via microwave-mediated Suzuki-Miyaura couplings. Many derivatives were crystallised from dichloromethane/methanol and analysed by single crystal X-ray diffraction. An interesting structure was obtained for N-(4'-methylbiphenyl-4-yl)acetamide with Z'=6 and hydrogen-bonding networks of the type N-H ··· O in the unit cell.
9272-9277
Baltus, Christine B.
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Press, Neil J.
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Antonijevic, Milan D.
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Tizzard, Graham J.
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Coles, Simon J.
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Spencer, John
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November 2012
Baltus, Christine B.
9345057c-8fc2-447d-aaf4-ee613ad4d131
Press, Neil J.
ee2e10f8-f371-4bf6-9c23-e385d0e16406
Antonijevic, Milan D.
b5c9b4dd-4e10-404c-b938-84a741b4e241
Tizzard, Graham J.
8474c0fa-40df-43a6-a662-7f3c4722dbf2
Coles, Simon J.
3116f58b-c30c-48cf-bdd5-397d1c1fecf8
Spencer, John
a3cf55cd-a4c7-4af6-b16c-96c8fb8c4cf4
Baltus, Christine B., Press, Neil J., Antonijevic, Milan D., Tizzard, Graham J., Coles, Simon J. and Spencer, John
(2012)
Synthesis of a biphenyl library for studies of hydrogen bonding in the solid state.
Tetrahedron, 68 (45), .
(doi:10.1016/j.tet.2012.08.062).
Abstract
A biphenyl library incorporating amide and sulfonamide groups has been synthesised via microwave-mediated Suzuki-Miyaura couplings. Many derivatives were crystallised from dichloromethane/methanol and analysed by single crystal X-ray diffraction. An interesting structure was obtained for N-(4'-methylbiphenyl-4-yl)acetamide with Z'=6 and hydrogen-bonding networks of the type N-H ··· O in the unit cell.
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Published date: November 2012
Organisations:
Organic Chemistry: Synthesis, Catalysis and Flow
Identifiers
Local EPrints ID: 346092
URI: http://eprints.soton.ac.uk/id/eprint/346092
ISSN: 0040-4020
PURE UUID: 95078a1b-b853-4be8-bd22-b012796746f4
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Date deposited: 19 Dec 2012 08:51
Last modified: 15 Mar 2024 03:10
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Contributors
Author:
Christine B. Baltus
Author:
Neil J. Press
Author:
Milan D. Antonijevic
Author:
John Spencer
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