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rac-N-{6-[Bromo(hydroxy)methyl]-2-pyridyl}pivalamide

rac-N-{6-[Bromo(hydroxy)methyl]-2-pyridyl}pivalamide
rac-N-{6-[Bromo(hydroxy)methyl]-2-pyridyl}pivalamide
The title compound, C(11)H(15)BrN(2)O(2), contains an amide group which is close to coplanar with the adjacent pyridine ring, the dihedral angle between the planes being 9.0 (5)degrees. The molecular packing reveals a mutual hydrogen-bond interaction between centrosymmetrically related hydroxyl O atoms. Further hydrogen bonding involving O-H center dot center dot center dot Br and N-H center dot center dot center dot Br interactions also appears to consolidate the packing.
o647
Knight, J.C.
856fc97c-953c-4928-b389-40cdce61c078
Saad, F.A.
697d5c82-d71c-4849-8eb2-b99fe3033964
Amoroso, A.J.
6a2d8b83-dea3-47ae-a0fa-d6d3b8f35cc5
Kariuki, B.M.
6accba33-4b48-4b54-9ee3-9abe182b731f
Coles, S.J.
3116f58b-c30c-48cf-bdd5-397d1c1fecf8
Knight, J.C.
856fc97c-953c-4928-b389-40cdce61c078
Saad, F.A.
697d5c82-d71c-4849-8eb2-b99fe3033964
Amoroso, A.J.
6a2d8b83-dea3-47ae-a0fa-d6d3b8f35cc5
Kariuki, B.M.
6accba33-4b48-4b54-9ee3-9abe182b731f
Coles, S.J.
3116f58b-c30c-48cf-bdd5-397d1c1fecf8

Knight, J.C., Saad, F.A., Amoroso, A.J., Kariuki, B.M. and Coles, S.J. (2009) rac-N-{6-[Bromo(hydroxy)methyl]-2-pyridyl}pivalamide. Acta Crystallographica Section E: Structure Reports Online, 65 (3), o647. (doi:10.1107/S1600536809006795).

Record type: Article

Abstract

The title compound, C(11)H(15)BrN(2)O(2), contains an amide group which is close to coplanar with the adjacent pyridine ring, the dihedral angle between the planes being 9.0 (5)degrees. The molecular packing reveals a mutual hydrogen-bond interaction between centrosymmetrically related hydroxyl O atoms. Further hydrogen bonding involving O-H center dot center dot center dot Br and N-H center dot center dot center dot Br interactions also appears to consolidate the packing.

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More information

Published date: March 2009
Organisations: Organic Chemistry: Synthesis, Catalysis and Flow

Identifiers

Local EPrints ID: 346360
URI: http://eprints.soton.ac.uk/id/eprint/346360
DOI: doi:10.1107/S1600536809006795
PURE UUID: 0e78821e-d6e8-4e0d-aa82-c0b9d7db9293
ORCID for S.J. Coles: ORCID iD orcid.org/0000-0001-8414-9272

Catalogue record

Date deposited: 18 Dec 2012 14:36
Last modified: 15 Mar 2024 03:01

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Contributors

Author: J.C. Knight
Author: F.A. Saad
Author: A.J. Amoroso
Author: B.M. Kariuki
Author: S.J. Coles ORCID iD

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