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Effect of 1-deoxy-d-lactose upon the crystallization ofd-lactose

Effect of 1-deoxy-d-lactose upon the crystallization ofd-lactose
Effect of 1-deoxy-d-lactose upon the crystallization ofd-lactose
The synthesis and crystal structure of 1-deoxy-D-lactose is described, as is its use as an additive in the crystallization Of D-lactose. This has resulted in the formation of alpha beta-D-lactose for the first time at room temperature. Single-crystal analysis shows differences between this analysis and the structure previously obtained from powder data, particularly in the hydrogen-bonding patterns.
1528-7483
3927-3934
Guiry, Kevin P.
008b1649-cb93-4ba2-8a69-2603ecf58143
Coles, Simon J.
3116f58b-c30c-48cf-bdd5-397d1c1fecf8
Moynihan, Humphrey A.
4eab6271-11cc-451e-abbf-09b030ee0f2e
Lawrence, Simon E.
9f9d8451-35de-4ee7-8c47-ed6e84748b56
Guiry, Kevin P.
008b1649-cb93-4ba2-8a69-2603ecf58143
Coles, Simon J.
3116f58b-c30c-48cf-bdd5-397d1c1fecf8
Moynihan, Humphrey A.
4eab6271-11cc-451e-abbf-09b030ee0f2e
Lawrence, Simon E.
9f9d8451-35de-4ee7-8c47-ed6e84748b56

Guiry, Kevin P., Coles, Simon J., Moynihan, Humphrey A. and Lawrence, Simon E. (2008) Effect of 1-deoxy-d-lactose upon the crystallization ofd-lactose. Crystal Growth & Design, 8 (11), 3927-3934. (doi:10.1021/cg070598n).

Record type: Article

Abstract

The synthesis and crystal structure of 1-deoxy-D-lactose is described, as is its use as an additive in the crystallization Of D-lactose. This has resulted in the formation of alpha beta-D-lactose for the first time at room temperature. Single-crystal analysis shows differences between this analysis and the structure previously obtained from powder data, particularly in the hydrogen-bonding patterns.

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More information

Published date: November 2008
Organisations: Organic Chemistry: Synthesis, Catalysis and Flow, Chemistry

Identifiers

Local EPrints ID: 346423
URI: http://eprints.soton.ac.uk/id/eprint/346423
ISSN: 1528-7483
PURE UUID: 680a2e09-27f3-441e-90e6-da14abe71ed7
ORCID for Simon J. Coles: ORCID iD orcid.org/0000-0001-8414-9272

Catalogue record

Date deposited: 20 Dec 2012 15:48
Last modified: 18 Feb 2021 16:53

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Contributors

Author: Kevin P. Guiry
Author: Simon J. Coles ORCID iD
Author: Humphrey A. Moynihan
Author: Simon E. Lawrence

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