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Channelled crystals formed by tubular stacking of a 4 + 4 phenylene-piperazine macrocycle

Channelled crystals formed by tubular stacking of a 4 + 4 phenylene-piperazine macrocycle
Channelled crystals formed by tubular stacking of a 4 + 4 phenylene-piperazine macrocycle
The 4 + 4 macrocycle{CH(2)C(6)H(4)CH(2)N(CH(2)CH(2))(2)N}(4) with alternating para-phenylene and piperazine groups linked by methylene spacers adopts tubular stacking in the crystal with 36% solvent-filled volume.
1466-8033
1048-1050
Dawson, Conor
fb2bd07e-d863-4963-9244-8b51ea2caa70
Horton, Peter N.
154c8930-bfc3-495b-ad4a-8a278d5da3a5
Hursthouse, Michael B.
57a2ddf9-b1b3-4f38-bfe9-ef2f526388da
James, Stuart L.
64b3fff6-707c-4523-823b-e4890ed07b18
Dawson, Conor
fb2bd07e-d863-4963-9244-8b51ea2caa70
Horton, Peter N.
154c8930-bfc3-495b-ad4a-8a278d5da3a5
Hursthouse, Michael B.
57a2ddf9-b1b3-4f38-bfe9-ef2f526388da
James, Stuart L.
64b3fff6-707c-4523-823b-e4890ed07b18

Dawson, Conor, Horton, Peter N., Hursthouse, Michael B. and James, Stuart L. (2010) Channelled crystals formed by tubular stacking of a 4 + 4 phenylene-piperazine macrocycle. CrystEngComm, 12 (4), 1048-1050. (doi:10.1039/b917953d).

Record type: Article

Abstract

The 4 + 4 macrocycle{CH(2)C(6)H(4)CH(2)N(CH(2)CH(2))(2)N}(4) with alternating para-phenylene and piperazine groups linked by methylene spacers adopts tubular stacking in the crystal with 36% solvent-filled volume.

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More information

Published date: 10 November 2010
Organisations: Organic Chemistry: Synthesis, Catalysis and Flow, Chemistry

Identifiers

Local EPrints ID: 347455
URI: http://eprints.soton.ac.uk/id/eprint/347455
ISSN: 1466-8033
PURE UUID: 41e5b2a6-3f10-4927-918c-c1125b7c0f5f
ORCID for Peter N. Horton: ORCID iD orcid.org/0000-0001-8886-2016

Catalogue record

Date deposited: 04 Feb 2013 16:04
Last modified: 31 Jul 2019 00:46

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