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Tetraphenylphosphonium octahydrotriborate

Tetraphenylphosphonium octahydrotriborate
Tetraphenylphosphonium octahydrotriborate
The structure of the title salt, C(24)H(20)P(+)center dot H(8)B(3)(-) , at 120 (2) K has triclinic (P1) symmetry with an unusual Z = 5, although there is pseudosymmetry observedwith the tetraphenylphosphonium cations exhibiting I (4) over bar symmetry. One of the anions is disordered over two sets of sites with refined occupancies of 0.478 (11) and 0.522 (11)
o833-o833
Beckett, Michael A.
5b021ef6-fa5c-4f6d-9998-3313558f0dc1
Horton, Peter N.
154c8930-bfc3-495b-ad4a-8a278d5da3a5
Hursthouse, Michael B.
57a2ddf9-b1b3-4f38-bfe9-ef2f526388da
Pszolla, Christian
e80ac47e-fafa-49ac-ab72-a6ef5469a76a
Beckett, Michael A.
5b021ef6-fa5c-4f6d-9998-3313558f0dc1
Horton, Peter N.
154c8930-bfc3-495b-ad4a-8a278d5da3a5
Hursthouse, Michael B.
57a2ddf9-b1b3-4f38-bfe9-ef2f526388da
Pszolla, Christian
e80ac47e-fafa-49ac-ab72-a6ef5469a76a

Beckett, Michael A., Horton, Peter N., Hursthouse, Michael B. and Pszolla, Christian (2010) Tetraphenylphosphonium octahydrotriborate. Acta Crystallographica Section E: Structure Reports Online, 66 (4), o833-o833. (doi:10.1107/S1600536810008263).

Record type: Article

Abstract

The structure of the title salt, C(24)H(20)P(+)center dot H(8)B(3)(-) , at 120 (2) K has triclinic (P1) symmetry with an unusual Z = 5, although there is pseudosymmetry observedwith the tetraphenylphosphonium cations exhibiting I (4) over bar symmetry. One of the anions is disordered over two sets of sites with refined occupancies of 0.478 (11) and 0.522 (11)

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Published date: April 2010
Organisations: Organic Chemistry: Synthesis, Catalysis and Flow

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Local EPrints ID: 347479
URI: http://eprints.soton.ac.uk/id/eprint/347479
DOI: doi:10.1107/S1600536810008263
PURE UUID: b5149842-ff1f-4c48-876f-58e1a002ff0b
ORCID for Peter N. Horton: ORCID iD orcid.org/0000-0001-8886-2016

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Date deposited: 23 Jan 2013 11:47
Last modified: 15 Mar 2024 03:04

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Contributors

Author: Michael A. Beckett
Author: Peter N. Horton ORCID iD
Author: Michael B. Hursthouse
Author: Christian Pszolla

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