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Synthesis of fumaramide derived [3]rotaxanes as potential precursors for molecular boxes

Synthesis of fumaramide derived [3]rotaxanes as potential precursors for molecular boxes
Synthesis of fumaramide derived [3]rotaxanes as potential precursors for molecular boxes
Three new fumaramide-derived [3]rotaxanes have been synthesized, with the aim of macrocycle linking to form a molecular box. In one case, a nine-component templated [3]rotaxane synthesis was accomplished in 40% yield. Rotaxane reduction resulted in an unexpectedly facile de-slipping process.
1359-7345
5010-5012
Simpkins, Nigel S.
87881fc0-efb0-4caa-85be-1e655785f939
Weske, Damian F.
5b49ced0-7369-4c86-8f14-b0de26a1d22a
Male, Louise
89b88c4f-2308-4b94-8f3a-2dc537a66533
Coles, Simon J.
3116f58b-c30c-48cf-bdd5-397d1c1fecf8
Pitak, Mateusz B.
eeb6a00f-2291-4376-830f-d30dfd607ed1
Simpkins, Nigel S.
87881fc0-efb0-4caa-85be-1e655785f939
Weske, Damian F.
5b49ced0-7369-4c86-8f14-b0de26a1d22a
Male, Louise
89b88c4f-2308-4b94-8f3a-2dc537a66533
Coles, Simon J.
3116f58b-c30c-48cf-bdd5-397d1c1fecf8
Pitak, Mateusz B.
eeb6a00f-2291-4376-830f-d30dfd607ed1

Simpkins, Nigel S., Weske, Damian F., Male, Louise, Coles, Simon J. and Pitak, Mateusz B. (2013) Synthesis of fumaramide derived [3]rotaxanes as potential precursors for molecular boxes. Chemical Communications, 49 (44), 5010-5012. (doi:10.1039/c3cc42045k).

Record type: Article

Abstract

Three new fumaramide-derived [3]rotaxanes have been synthesized, with the aim of macrocycle linking to form a molecular box. In one case, a nine-component templated [3]rotaxane synthesis was accomplished in 40% yield. Rotaxane reduction resulted in an unexpectedly facile de-slipping process.

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More information

Published date: 2013
Organisations: Organic Chemistry: Synthesis, Catalysis and Flow, Chemistry, Faculty of Natural and Environmental Sciences

Identifiers

Local EPrints ID: 362498
URI: http://eprints.soton.ac.uk/id/eprint/362498
ISSN: 1359-7345
PURE UUID: f9d742f1-899c-4047-9467-7d52726d2838
ORCID for Simon J. Coles: ORCID iD orcid.org/0000-0001-8414-9272
ORCID for Mateusz B. Pitak: ORCID iD orcid.org/0000-0002-3680-7100

Catalogue record

Date deposited: 26 Feb 2014 11:34
Last modified: 18 Feb 2021 16:53

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Contributors

Author: Nigel S. Simpkins
Author: Damian F. Weske
Author: Louise Male
Author: Simon J. Coles ORCID iD
Author: Mateusz B. Pitak ORCID iD

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