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Synthesis and structural characterisation of hydrogenous and transition metal framework materials

Synthesis and structural characterisation of hydrogenous and transition metal framework materials
Synthesis and structural characterisation of hydrogenous and transition metal framework materials
In this work, inorganic framework materials, with structures based on copper polyhedra and anionic species including (fluoro)-phosphate tetrahedra and F-/CL-, have been synthesised and fully characterised. These materials were produced through the application of hydrothermal techniques, with the single crystal X-ray diffraction utilised as the principal characterisation technique, supported by X-ray and neutron powder diffraction, thermogravimetric analysis and scanning electron microscopy with energy dispersive X-ray analysis.
Williams, Edward R.
f0b6c85a-f747-4957-8f3d-959eea6d7efb
Williams, Edward R.
f0b6c85a-f747-4957-8f3d-959eea6d7efb
WALES, DOMINIC J
c001ff27-d3ac-4d2e-859f-9e963fc0374c

(2013) Synthesis and structural characterisation of hydrogenous and transition metal framework materials. University of Southampton, Chemistry, Doctoral Thesis, 317pp.

Record type: Thesis (Doctoral)

Abstract

In this work, inorganic framework materials, with structures based on copper polyhedra and anionic species including (fluoro)-phosphate tetrahedra and F-/CL-, have been synthesised and fully characterised. These materials were produced through the application of hydrothermal techniques, with the single crystal X-ray diffraction utilised as the principal characterisation technique, supported by X-ray and neutron powder diffraction, thermogravimetric analysis and scanning electron microscopy with energy dispersive X-ray analysis.

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Published date: 31 August 2013
Organisations: University of Southampton, Chemistry

Identifiers

Local EPrints ID: 366988
URI: http://eprints.soton.ac.uk/id/eprint/366988
PURE UUID: cb09ea12-1df2-41b2-b6dd-60d5c8287067

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Date deposited: 22 Oct 2014 10:52
Last modified: 18 Jul 2017 02:05

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Contributors

Author: Edward R. Williams
Thesis advisor: DOMINIC J WALES

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