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Microstructure and mechanical properties of physical vapor deposited Cu/W nanoscale multilayers: influence of layer thickness and temperature

Microstructure and mechanical properties of physical vapor deposited Cu/W nanoscale multilayers: influence of layer thickness and temperature
Microstructure and mechanical properties of physical vapor deposited Cu/W nanoscale multilayers: influence of layer thickness and temperature
Based on our previous knowledge on Cu/Nb nanoscale metallic multilayers (NMMs), Cu/W NMMs show a good potential for applications as heat skins in plasma experiments and armors, and it could be expected that the substitution of Nb by W would increase the strength, particularly at high temperatures. To check this hypothesis, Cu/W NMMs with individual layer thicknesses ranging between 5 and 30 nm were deposited by physical vapor deposition, and their mechanical properties were measured by nanoindentation. The results showed that, contrary to Cu/Nb NMMs, the hardness was independent of the layer thickness and decreased rapidly with temperature, especially above 200 °C. This behavior was attributed to the growth morphology of the W layers as well as the jagged Cu/W interface, both a consequence of the low W adatom mobility during deposition. Therefore, future efforts on the development of Cu/W multilayers should concentrate on optimization of the W deposition parameters via substrate heating and/or ion assisted deposition to increase the W adatom mobility during deposition
copper–tungsten multilayers, mechanical properties, microstructure, hot hardness
0040-6090
275-282
Monclus, M. A.
0dae16e5-baf8-4fca-b5e1-996a91bd9de8
Karlik, M.
26f74a9e-c3e3-4f97-8f8d-32a8a6f288a2
Callisti, M.
093b5320-2398-4d72-8b09-278d22a08937
Frutos, E.
8730c6ea-7f59-44b7-aa33-cfee57de8b25
LLorka, J.
edf805ff-da22-4941-961f-8613f8383138
Polcar, T.
c669b663-3ba9-4e7b-9f97-8ef5655ac6d2
Molina-Aldareguía, J.M.
45f43d07-9207-44e8-bf48-c61604aa1e70
Monclus, M. A.
0dae16e5-baf8-4fca-b5e1-996a91bd9de8
Karlik, M.
26f74a9e-c3e3-4f97-8f8d-32a8a6f288a2
Callisti, M.
093b5320-2398-4d72-8b09-278d22a08937
Frutos, E.
8730c6ea-7f59-44b7-aa33-cfee57de8b25
LLorka, J.
edf805ff-da22-4941-961f-8613f8383138
Polcar, T.
c669b663-3ba9-4e7b-9f97-8ef5655ac6d2
Molina-Aldareguía, J.M.
45f43d07-9207-44e8-bf48-c61604aa1e70

Monclus, M. A., Karlik, M., Callisti, M., Frutos, E., LLorka, J., Polcar, T. and Molina-Aldareguía, J.M. (2014) Microstructure and mechanical properties of physical vapor deposited Cu/W nanoscale multilayers: influence of layer thickness and temperature. Thin Solid Films, 571 (2), 275-282. (doi:10.1016/j.tsf.2014.05.044).

Record type: Article

Abstract

Based on our previous knowledge on Cu/Nb nanoscale metallic multilayers (NMMs), Cu/W NMMs show a good potential for applications as heat skins in plasma experiments and armors, and it could be expected that the substitution of Nb by W would increase the strength, particularly at high temperatures. To check this hypothesis, Cu/W NMMs with individual layer thicknesses ranging between 5 and 30 nm were deposited by physical vapor deposition, and their mechanical properties were measured by nanoindentation. The results showed that, contrary to Cu/Nb NMMs, the hardness was independent of the layer thickness and decreased rapidly with temperature, especially above 200 °C. This behavior was attributed to the growth morphology of the W layers as well as the jagged Cu/W interface, both a consequence of the low W adatom mobility during deposition. Therefore, future efforts on the development of Cu/W multilayers should concentrate on optimization of the W deposition parameters via substrate heating and/or ion assisted deposition to increase the W adatom mobility during deposition

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More information

Published date: 28 November 2014
Keywords: copper–tungsten multilayers, mechanical properties, microstructure, hot hardness
Organisations: nCATS Group

Identifiers

Local EPrints ID: 373322
URI: http://eprints.soton.ac.uk/id/eprint/373322
ISSN: 0040-6090
PURE UUID: effee3a3-0f89-490c-8dfe-0bb689288d9b
ORCID for T. Polcar: ORCID iD orcid.org/0000-0002-0863-6287

Catalogue record

Date deposited: 14 Jan 2015 17:25
Last modified: 15 Mar 2024 03:40

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Contributors

Author: M. A. Monclus
Author: M. Karlik
Author: M. Callisti
Author: E. Frutos
Author: J. LLorka
Author: T. Polcar ORCID iD
Author: J.M. Molina-Aldareguía

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