The University of Southampton
University of Southampton Institutional Repository

Towards microfluidic reactors for in situ synchrotron infrared studies

Towards microfluidic reactors for in situ synchrotron infrared studies
Towards microfluidic reactors for in situ synchrotron infrared studies
Anodically bonded etched siliconmicrofluidic devices that allow infrared spectroscopic measurement of solutions are reported. These extend spatially well-resolved in situ infrared measurement to higher temperatures and pressures than previously reported, making them useful for effectively time-resolved measurement of realistic catalytic processes. A data processing technique necessary for the mitigation of interference fringes caused by multiple reflections of the probe beam is also described
0034-6748
24101
Silverwood, I.P.
0e986985-be71-4665-8ccc-35a0a35e044c
Al-Rifai, N.
c1651d17-deeb-4704-8161-befb3be79eb4
Cao, E.
eb7a2cac-afd2-424a-ad56-79029d7a7e00
Nelson, D.J.
0d973cdb-9745-47c7-83fe-7de3679d7694
Chutia, A.
ca6c0244-cc7f-481a-840b-a950cbcfc7e7
Wells, Peter
bc4fdc2d-a490-41bf-86cc-400edecf2266
Nolan, S.P.
10f56967-c5a5-4bbf-b848-6cbf8b1d8720
Frogley, M.D.
c218cf97-0df9-4a78-8b7a-42864748caac
Cinque, G.
f5655993-a290-4ebb-bfcc-639af87125f3
Gavriilidis, A.
8284f19c-ba83-442d-b78f-ee610486a5be
Catlow, C.R.A.
e7bf93ac-edd4-4a53-86df-11199f1639e9
Silverwood, I.P.
0e986985-be71-4665-8ccc-35a0a35e044c
Al-Rifai, N.
c1651d17-deeb-4704-8161-befb3be79eb4
Cao, E.
eb7a2cac-afd2-424a-ad56-79029d7a7e00
Nelson, D.J.
0d973cdb-9745-47c7-83fe-7de3679d7694
Chutia, A.
ca6c0244-cc7f-481a-840b-a950cbcfc7e7
Wells, Peter
bc4fdc2d-a490-41bf-86cc-400edecf2266
Nolan, S.P.
10f56967-c5a5-4bbf-b848-6cbf8b1d8720
Frogley, M.D.
c218cf97-0df9-4a78-8b7a-42864748caac
Cinque, G.
f5655993-a290-4ebb-bfcc-639af87125f3
Gavriilidis, A.
8284f19c-ba83-442d-b78f-ee610486a5be
Catlow, C.R.A.
e7bf93ac-edd4-4a53-86df-11199f1639e9

Silverwood, I.P., Al-Rifai, N., Cao, E., Nelson, D.J., Chutia, A., Wells, Peter, Nolan, S.P., Frogley, M.D., Cinque, G., Gavriilidis, A. and Catlow, C.R.A. (2016) Towards microfluidic reactors for in situ synchrotron infrared studies. Review of Scientific Instruments, 87 (2), 24101. (doi:10.1063/1.4941825).

Record type: Article

Abstract

Anodically bonded etched siliconmicrofluidic devices that allow infrared spectroscopic measurement of solutions are reported. These extend spatially well-resolved in situ infrared measurement to higher temperatures and pressures than previously reported, making them useful for effectively time-resolved measurement of realistic catalytic processes. A data processing technique necessary for the mitigation of interference fringes caused by multiple reflections of the probe beam is also described

Other
1.4941825.pdf_expires=1474281313&id=id&accname=2103930&checksum=36E38AFBCD5A899DB1D368E9A4180BC2 - Version of Record
Download (1MB)

More information

Accepted/In Press date: 28 January 2016
Published date: 19 February 2016
Organisations: Organic Chemistry: SCF

Identifiers

Local EPrints ID: 400551
URI: http://eprints.soton.ac.uk/id/eprint/400551
ISSN: 0034-6748
PURE UUID: c6c786d7-b0f1-4a22-9726-c6f60fd47451
ORCID for Peter Wells: ORCID iD orcid.org/0000-0002-0859-9172

Catalogue record

Date deposited: 19 Sep 2016 10:23
Last modified: 15 Mar 2024 03:24

Export record

Altmetrics

Contributors

Author: I.P. Silverwood
Author: N. Al-Rifai
Author: E. Cao
Author: D.J. Nelson
Author: A. Chutia
Author: Peter Wells ORCID iD
Author: S.P. Nolan
Author: M.D. Frogley
Author: G. Cinque
Author: A. Gavriilidis
Author: C.R.A. Catlow

Download statistics

Downloads from ePrints over the past year. Other digital versions may also be available to download e.g. from the publisher's website.

View more statistics

Atom RSS 1.0 RSS 2.0

Contact ePrints Soton: eprints@soton.ac.uk

ePrints Soton supports OAI 2.0 with a base URL of http://eprints.soton.ac.uk/cgi/oai2

This repository has been built using EPrints software, developed at the University of Southampton, but available to everyone to use.

We use cookies to ensure that we give you the best experience on our website. If you continue without changing your settings, we will assume that you are happy to receive cookies on the University of Southampton website.

×