This data file contains the information about the figure 6,figure 7 a,figure 7 b figure 8, figure 9, figure 10, figure 11 Figure 6 Raman spectra of the TiNS/ PbO2/RVC obtained by anodic electrophoretic deposition a) calcined and b) non-calcined at 450 ºC. Figure 7 a Polarization curve by using coating 1) (TiNS /PbO2 / RVC) as anode after calcination at 450 ºC in 0.5 mol L-1 Na2SO4, pH=3.0. 2) (PbO2 / RVC) as anode in 0.5 mol L-1 Na2SO4, Experimental conditions: Potential sweep rate = 10 mV s-1 , temperature: 298 K. Figure 7 b Polarization curve by using novel coating 1) (TiNS /PbO2 / RVC) as anode in an electrolyte 10 ppm R.B-5 dye in 0.5 mol L-1 Na2SO4, pH=3.0. 2) (PbO2 / RVC) as anode after calcination at 450 ºC in an electrolyte 10 ppm R.B-5 dye in 0.5 mol L-1 Na2SO4, pH=3.0, Experimental conditions: Potential sweep rate = 10 mV s-1, Temperature: 298 K. Figure 8 Electrochemical remediation of RB-5 dye by ¦) RVC, ?) Photoassisted fenton using Iron oxide on activated alumina support [49], ?) RVC/PbO2, and ?) calcined TiNS/PbO2/RVC. Figure 9 Electrochemical remediation kinetics of RB-5 dye by ¦) RVC, ?) Photoassisted fenton using Iron oxide on activated alumina support [49],?) RVC/PbO2, and?) calcined TiNS/PbO2/RVC. Figure 10 Photocatalytic remediation of RB-5 dye by ?) RVC ?) calcined TiNS/PbO2/RVC Figure 11 Photocatalytic remediation kinetics by ?) RVC ?) calcined TiNS/PbO2/RVC