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Using GISAXS to detect correlations between the locations of gold particles electrodeposited from aqueous solution

Using GISAXS to detect correlations between the locations of gold particles electrodeposited from aqueous solution
Using GISAXS to detect correlations between the locations of gold particles electrodeposited from aqueous solution
Electrodeposition is a powerful tool for the bottom up fabrication of novel electronic devices. This necessitates complete understanding of the deposition process beyond the classical description using current transients. Recent calculations predict deviations within the spatial arrangement of electrodeposited particles, away from random nucleation. The spatial arrangement of Au particles generated through aqueous electrodeposition on a non-templated substrate is investigated by Grazing Incidence Small Angle X-ray Scattering (GISAXS). We show that GISAXS is able to reveal spatial correlations within deposited particles which are not easily detectable by microscopy.
0743-7463
Moehl, Gilles, Ernest Heinrich Karl
c3f40572-28c6-4467-a118-502000132f8c
Bartlett, Philip N.
d99446db-a59d-4f89-96eb-f64b5d8bb075
Hector, Andrew L.
f19a8f31-b37f-4474-b32a-b7cf05b9f0e5
Moehl, Gilles, Ernest Heinrich Karl
c3f40572-28c6-4467-a118-502000132f8c
Bartlett, Philip N.
d99446db-a59d-4f89-96eb-f64b5d8bb075
Hector, Andrew L.
f19a8f31-b37f-4474-b32a-b7cf05b9f0e5

Moehl, Gilles, Ernest Heinrich Karl, Bartlett, Philip N. and Hector, Andrew L. (2020) Using GISAXS to detect correlations between the locations of gold particles electrodeposited from aqueous solution. Langmuir. (doi:10.1021/acs.langmuir.9b03400).

Record type: Article

Abstract

Electrodeposition is a powerful tool for the bottom up fabrication of novel electronic devices. This necessitates complete understanding of the deposition process beyond the classical description using current transients. Recent calculations predict deviations within the spatial arrangement of electrodeposited particles, away from random nucleation. The spatial arrangement of Au particles generated through aqueous electrodeposition on a non-templated substrate is investigated by Grazing Incidence Small Angle X-ray Scattering (GISAXS). We show that GISAXS is able to reveal spatial correlations within deposited particles which are not easily detectable by microscopy.

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Accepted/In Press date: 2 April 2020
e-pub ahead of print date: 2 April 2020

Identifiers

Local EPrints ID: 439205
URI: http://eprints.soton.ac.uk/id/eprint/439205
ISSN: 0743-7463
PURE UUID: bea8a779-30b9-45ec-9fad-c9c2b4775ad5
ORCID for Philip N. Bartlett: ORCID iD orcid.org/0000-0002-7300-6900
ORCID for Andrew L. Hector: ORCID iD orcid.org/0000-0002-9964-2163

Catalogue record

Date deposited: 07 Apr 2020 16:30
Last modified: 02 Apr 2021 04:01

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