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Triethyl ammonium salt of O,O'-bis(p-tolyl)dithiophosphate, [Et3NH](+)[(4-MeC6H4O)(2)PS2](-)

Triethyl ammonium salt of O,O'-bis(p-tolyl)dithiophosphate, [Et3NH](+)[(4-MeC6H4O)(2)PS2](-)
Triethyl ammonium salt of O,O'-bis(p-tolyl)dithiophosphate, [Et3NH](+)[(4-MeC6H4O)(2)PS2](-)
Triethyl ammonium Salt of O,O'-bis(p-tolyl)dithiophosphate and O,O'-bis(m-tolyl)dithiophosphate have been obtained by reaction of p- and m-cresol, respectively with P2S5 in toluene and have been characterized by elemental analysis, IR, H-1 and P-31 NMR spectroscopy. The molecular structure of O,O'-bis(p-tolyl)dithiophosphate has been determined. Crystal data: [Et3NH](+)[(4-MeC6H4O)(2)PS2](-): Monoclinic, P2(1)/c, a=15.2441(9) angstrom, b=10.415(2) angstrom, c=3.9726(9) angstrom, beta=91.709(7)degrees, V=2217.5(1)angstrom(-3), Z=4.
1074-1542
627-630
Bingham, A.L.
8349446d-f3ab-4a2c-9b7b-88b01a9f59c0
Drake, J.E.
cf5a2c45-a2cb-4361-8b31-f2295e2050b7
Gurnani, C.
05167fec-a511-4087-842c-ff8d69bdf91c
Hursthouse, M.B.
57a2ddf9-b1b3-4f38-bfe9-ef2f526388da
Light, M.E.
cf57314e-6856-491b-a8d2-2dffc452e161
Nirwan, M.
3075fd5e-d99a-421d-bf72-20624f97d8fe
Ratnani, R.
5c33e340-5b43-4fae-b43d-c37ae26100ff
Bingham, A.L.
8349446d-f3ab-4a2c-9b7b-88b01a9f59c0
Drake, J.E.
cf5a2c45-a2cb-4361-8b31-f2295e2050b7
Gurnani, C.
05167fec-a511-4087-842c-ff8d69bdf91c
Hursthouse, M.B.
57a2ddf9-b1b3-4f38-bfe9-ef2f526388da
Light, M.E.
cf57314e-6856-491b-a8d2-2dffc452e161
Nirwan, M.
3075fd5e-d99a-421d-bf72-20624f97d8fe
Ratnani, R.
5c33e340-5b43-4fae-b43d-c37ae26100ff

Bingham, A.L., Drake, J.E., Gurnani, C., Hursthouse, M.B., Light, M.E., Nirwan, M. and Ratnani, R. (2006) Triethyl ammonium salt of O,O'-bis(p-tolyl)dithiophosphate, [Et3NH](+)[(4-MeC6H4O)(2)PS2](-). Journal of Chemical Crystallography, 36 (10), 627-630. (doi:10.1007/s10870-006-9107-3).

Record type: Article

Abstract

Triethyl ammonium Salt of O,O'-bis(p-tolyl)dithiophosphate and O,O'-bis(m-tolyl)dithiophosphate have been obtained by reaction of p- and m-cresol, respectively with P2S5 in toluene and have been characterized by elemental analysis, IR, H-1 and P-31 NMR spectroscopy. The molecular structure of O,O'-bis(p-tolyl)dithiophosphate has been determined. Crystal data: [Et3NH](+)[(4-MeC6H4O)(2)PS2](-): Monoclinic, P2(1)/c, a=15.2441(9) angstrom, b=10.415(2) angstrom, c=3.9726(9) angstrom, beta=91.709(7)degrees, V=2217.5(1)angstrom(-3), Z=4.

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Published date: 2006

Identifiers

Local EPrints ID: 44384
URI: https://eprints.soton.ac.uk/id/eprint/44384
ISSN: 1074-1542
PURE UUID: 9c479bb7-6263-4d16-a2a6-5ece47bfad5b
ORCID for M.E. Light: ORCID iD orcid.org/0000-0002-0585-0843

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Date deposited: 05 Mar 2007
Last modified: 14 Mar 2019 01:48

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