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Distance measurements in disodium ATP hydrates by means of P-31 double quantum two-dimensional solid-state NMR spectroscopy

Distance measurements in disodium ATP hydrates by means of P-31 double quantum two-dimensional solid-state NMR spectroscopy
Distance measurements in disodium ATP hydrates by means of P-31 double quantum two-dimensional solid-state NMR spectroscopy
POST-C7 measurements provide constraints allowing distinguishing crystal lattice organization and establishing intra and/or intermolecular distances between phosphorus atoms of triphosphate chains for different hydrates of disodium ATP salts. Double-quantum efficiency in function of excitation time obtained from series of two-dimensional spectra for POST-C7 experiments was used to set up of buildup curves and semi-quantitative measure of P-31-P-31 length.
double-quantum nmr, 2d nmr correlation spectroscopy, post-c7, atp hydrates chemical-shift tensors, adenosine 5'-triphosphate, crystal, c-13, transition, trihydrate, humidity, sequence, model, acid
173-181
Potrzebowski, M.J.
7fc54c76-4b4b-41a6-9a43-16ce582bae68
Gajda, J.
198b593b-3562-4521-a064-b9c642335f9c
Ciesielski, W.
ea1ee254-89e2-47c7-a5bd-57fc37c07890
Montesinos, I.M.
48c74526-bdcb-44ab-bff8-07d21e6e5d10
Potrzebowski, M.J.
7fc54c76-4b4b-41a6-9a43-16ce582bae68
Gajda, J.
198b593b-3562-4521-a064-b9c642335f9c
Ciesielski, W.
ea1ee254-89e2-47c7-a5bd-57fc37c07890
Montesinos, I.M.
48c74526-bdcb-44ab-bff8-07d21e6e5d10

Potrzebowski, M.J., Gajda, J., Ciesielski, W. and Montesinos, I.M. (2006) Distance measurements in disodium ATP hydrates by means of P-31 double quantum two-dimensional solid-state NMR spectroscopy. Journal of Magnetic Resonance, 179 (2), 173-181. (doi:10.1016/j.jmr.2005.11.016).

Record type: Article

Abstract

POST-C7 measurements provide constraints allowing distinguishing crystal lattice organization and establishing intra and/or intermolecular distances between phosphorus atoms of triphosphate chains for different hydrates of disodium ATP salts. Double-quantum efficiency in function of excitation time obtained from series of two-dimensional spectra for POST-C7 experiments was used to set up of buildup curves and semi-quantitative measure of P-31-P-31 length.

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More information

Published date: 2006
Keywords: double-quantum nmr, 2d nmr correlation spectroscopy, post-c7, atp hydrates chemical-shift tensors, adenosine 5'-triphosphate, crystal, c-13, transition, trihydrate, humidity, sequence, model, acid

Identifiers

Local EPrints ID: 44527
URI: http://eprints.soton.ac.uk/id/eprint/44527
PURE UUID: 51d1089c-8c9c-48b4-a8f2-a8ec2a909e7a

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Date deposited: 07 Mar 2007
Last modified: 13 Mar 2019 21:07

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