READ ME File For 'Electronic Data: Toward sustainable syntheses of Ca-based MOFs'

Dataset DOI: 10.5258/SOTON/D1926

ReadMe Author: Tom S. Crickmore, University of Southampton [orcid.org/0000-0001-7564-2700]

This dataset supports the publication:
AUTHORS: Tom. S. Crickmore, Haamidah Begum Sana, Hannah Mitchell, Molly Clark and Darren Bradshaw
TITLE:Toward sustainable syntheses of Ca-based MOFs
JOURNAL: Chemical Communications
PAPER DOI IF KNOWN: 10.1039/D1CC04032D 


This dataset contains: PXRD, TGA, FTIR, SEM, microscope images, digital images and NMR datasets relating to the above publication.

*CaBDC_PXRD.csv - PXRD data relating to Ca(BDC)(H2O)3 
*CaBDC_TGA.csv - TGA data relating to Ca(BDC)(H2O)3 
*CaFU_PXRD.csv - PXRD data relating to Ca(FU)(H2O)3
*CaFU_TGA.csv - TGA data relating to Ca(FU)(H2O)3
*CaSQ_BM_CO2-ads.csv - CO2 adsorption data at 298 K for Ca(SQ)(H2O) prepared via ball-milling
*CaSQ_eggshell_CO2-ads - CO2 adsorption data at 298 K for Ca(SQ)(H2O) prepared from eggshell
*CaSQ_Reference-mat_CO2-ads.csv - CO2 adsorption data at 298 K for Ca(SQ)(H2O) prepared from literature
*CaSQ_PXRD - PXRD data relating to Ca(SQ)(H2O)
*CaSQ_TGA - TGA data relating to Ca(SQ)(H2O)
*Precursor_FTIR.csv - FTIR data relating to precursors
*Precursor_PXRD.csv - PXRD data relating to precursors
*Precursor_TGA.csv - TGA data relating to precursors
*Reclaimed-H2BDC-NMR.zip - Zip file containing raw NMR data.
*1_inset.jpg - image of Ca(SQ)(H2O) crystals on an eggshell
*1_right.jpg - SEM of Ca(SQ)(H2O) on an eggshell
*2_1.tif - SEM of Ca(BDC)(H2O)3 prepared mechanochemically from calcite and reclaimed H2BDC
*2_2.tif - SEM of Ca(BDC)(H2O)3 prepared mechanochemically from eggshells and reclaimed H2BDC
*S1.png - crystal structure images of the three MOFs
*S3.jpg - SEM of Ca(SQ)(H2O) prepared in aqueous solution
*S4.jpg - image of crystals of Ca(FU)(H2O)3 prepared hydrothermally
*S6.tif - SEM of Ca(FU)(H2O)3 prepared mechanochemically from eggshells and H2FU
*S9_1.jpg - image of recycled PET bottle cut into small pieces
*S9_2.jpg - image of egghshells ground to varying degrees.
S13_1.jpg - SEM of eggshells
S13_2.jpg - SEM of eggshells
S14.jpg - image of Ca(SQ)(H2O) crystals viewed under a light microscope. Magnification x80. 
S15.jpg - image of Ca(SQ)(H2O) grown on eggshell. Membrane intact. 
S16_1.jpg - SEM image of Ca(SQ)(H2O) on eggshell. Membrane intact. 
S16_2.jpg - SEM image of Ca(SQ)(H2O) on eggshell. Membrane intact. 
S18.tif - SEM of Ca(SQ)(H2O) prepared mechanochemically from calcite and H2SQ
S26_1.png - asymmetric unit of H2BDC
S26_2.png - crystal packing of H2BDC 

Date that the file was created: 18 Aug, 2021