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Design of experiment study of the seeding of magnesium sulfate solutions

Design of experiment study of the seeding of magnesium sulfate solutions
Design of experiment study of the seeding of magnesium sulfate solutions

Statistical Design of Experiment methods have been used to investigate 24 seeding parameters in over a thousand crystallization cycles. Surprisingly, the mass or surface area of seeds were of no consequence. Only the method of stirring and the reuse of vessels were significant. We explain these results in terms of the single event and embryo coagulation mechanisms.

1528-7483
3613-3624
Coles, S. J.
3116f58b-c30c-48cf-bdd5-397d1c1fecf8
Robinson, D. I.
dcef4b3b-ac9b-4c1b-b8b2-1bee4b81a8cc
Davesne, A.
fbd36d7b-8222-4a7f-afac-724b7015343d
Threlfall, T. L.
6c670746-9730-49fc-9381-e45ae4807450
Coles, S. J.
3116f58b-c30c-48cf-bdd5-397d1c1fecf8
Robinson, D. I.
dcef4b3b-ac9b-4c1b-b8b2-1bee4b81a8cc
Davesne, A.
fbd36d7b-8222-4a7f-afac-724b7015343d
Threlfall, T. L.
6c670746-9730-49fc-9381-e45ae4807450

Coles, S. J., Robinson, D. I., Davesne, A. and Threlfall, T. L. (2022) Design of experiment study of the seeding of magnesium sulfate solutions. Crystal Growth and Design, 22 (6), 3613-3624. (doi:10.1021/acs.cgd.1c01257).

Record type: Article

Abstract

Statistical Design of Experiment methods have been used to investigate 24 seeding parameters in over a thousand crystallization cycles. Surprisingly, the mass or surface area of seeds were of no consequence. Only the method of stirring and the reuse of vessels were significant. We explain these results in terms of the single event and embryo coagulation mechanisms.

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Accepted/In Press date: 9 May 2022
e-pub ahead of print date: 9 May 2022
Published date: 1 June 2022
Additional Information: Publisher Copyright: © 2022 American Chemical Society. All rights reserved.

Identifiers

Local EPrints ID: 468449
URI: http://eprints.soton.ac.uk/id/eprint/468449
ISSN: 1528-7483
PURE UUID: 450a974f-7638-403a-bdf7-c5217db45496
ORCID for S. J. Coles: ORCID iD orcid.org/0000-0001-8414-9272

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Date deposited: 15 Aug 2022 17:01
Last modified: 16 Aug 2022 01:35

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Contributors

Author: S. J. Coles ORCID iD
Author: D. I. Robinson
Author: A. Davesne
Author: T. L. Threlfall

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