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Individual effect of recrystallisation nucleation sites on texture weakening in a magnesium alloy: Part 1-double twins

Individual effect of recrystallisation nucleation sites on texture weakening in a magnesium alloy: Part 1-double twins
Individual effect of recrystallisation nucleation sites on texture weakening in a magnesium alloy: Part 1-double twins
Recrystallised grain nucleation, grain growth and corresponding texture evolution in a cold-rolled rare earth containing WE43 Mg alloy during annealing at 490 °C was fully tracked using a quasi-in-situ electron backscatter diffraction method. The results show nucleation sites, such as double twins, can weaken the deformed texture and for the first time provide direct evidence that recrystallised grains originating from double twins can form the rare earth texture during annealing. Precipitation and recrystallisation occurred concurrently during most of the annealing period, with precipitates forming preferentially along prior grain and twin boundaries. These precipitates effectively retard the recrystallisation due to particle pinning leading to an excessively long time for the completion of recrystallisation. A large portion of recrystallised grains were observed to have 〈0001〉 poles tilted 20–45° away from the normal direction. The RE texture emerges during the nucleation of recrystallised grains and is maintained during subsequent uniform grain growth, which results in a stable RE texture being developed as recrystallisation progresses. The uniform grain growth could be attributed to solute drag suppressing the grain boundary mobility of those grains that had recrystallised with a basal texture and precipitate pinning restricting potential orientated grain growth.
Magnesium alloy, Recrystallisation, Deformation twin, Texture evolution, Precipitation
1359-6454
14-24
Guan, Dikai
d20c4acc-342a-43fa-a204-7283f0cc33bf
Rainforth, W. Mark
7226983c-4ca1-4f0a-8191-02e3424dc98f
Gao, Junheng
ff08c8df-b051-4ab1-bc03-3b6d68ab9d2e
Sharp, Joanne
0c691a1a-d13e-4e3b-92a1-9586f2b9e181
Wynne, Brad
778dc107-b462-47de-8054-cfa0556ea1df
Ma, Le
1b333b75-1734-4e63-a7d1-ca850ddc78fb
Guan, Dikai
d20c4acc-342a-43fa-a204-7283f0cc33bf
Rainforth, W. Mark
7226983c-4ca1-4f0a-8191-02e3424dc98f
Gao, Junheng
ff08c8df-b051-4ab1-bc03-3b6d68ab9d2e
Sharp, Joanne
0c691a1a-d13e-4e3b-92a1-9586f2b9e181
Wynne, Brad
778dc107-b462-47de-8054-cfa0556ea1df
Ma, Le
1b333b75-1734-4e63-a7d1-ca850ddc78fb

Guan, Dikai, Rainforth, W. Mark, Gao, Junheng, Sharp, Joanne, Wynne, Brad and Ma, Le (2017) Individual effect of recrystallisation nucleation sites on texture weakening in a magnesium alloy: Part 1-double twins. Acta Materialia, 135, 14-24. (doi:10.1016/j.actamat.2017.06.015).

Record type: Article

Abstract

Recrystallised grain nucleation, grain growth and corresponding texture evolution in a cold-rolled rare earth containing WE43 Mg alloy during annealing at 490 °C was fully tracked using a quasi-in-situ electron backscatter diffraction method. The results show nucleation sites, such as double twins, can weaken the deformed texture and for the first time provide direct evidence that recrystallised grains originating from double twins can form the rare earth texture during annealing. Precipitation and recrystallisation occurred concurrently during most of the annealing period, with precipitates forming preferentially along prior grain and twin boundaries. These precipitates effectively retard the recrystallisation due to particle pinning leading to an excessively long time for the completion of recrystallisation. A large portion of recrystallised grains were observed to have 〈0001〉 poles tilted 20–45° away from the normal direction. The RE texture emerges during the nucleation of recrystallised grains and is maintained during subsequent uniform grain growth, which results in a stable RE texture being developed as recrystallisation progresses. The uniform grain growth could be attributed to solute drag suppressing the grain boundary mobility of those grains that had recrystallised with a basal texture and precipitate pinning restricting potential orientated grain growth.

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More information

Published date: 15 August 2017
Keywords: Magnesium alloy, Recrystallisation, Deformation twin, Texture evolution, Precipitation

Identifiers

Local EPrints ID: 475006
URI: http://eprints.soton.ac.uk/id/eprint/475006
ISSN: 1359-6454
PURE UUID: cc87389d-bcd7-4dde-add4-22ddbc78830b
ORCID for Dikai Guan: ORCID iD orcid.org/0000-0002-3953-2878

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Date deposited: 08 Mar 2023 17:54
Last modified: 17 Mar 2024 04:17

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Contributors

Author: Dikai Guan ORCID iD
Author: W. Mark Rainforth
Author: Junheng Gao
Author: Joanne Sharp
Author: Brad Wynne
Author: Le Ma

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