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2-(2,7-Bis(pyridin-3-ylethynyl)fluoren-9-ylidene)malononitrile

2-(2,7-Bis(pyridin-3-ylethynyl)fluoren-9-ylidene)malononitrile
2-(2,7-Bis(pyridin-3-ylethynyl)fluoren-9-ylidene)malononitrile
The 2-(2,7-bis(pyridin-3-ylethynyl)fluoren-9-ylidene)malononitrile (1) was synthesized by reaction of 2,7-bis(pyridin-3-ylethynyl)fluoren-9-one with malononitrile in DMSO solution. The structural characterization of 1 by SC-XRD analysis was accompanied by elemental analysis, FT-IR, NMR, and MS measurements.
fluoren-9-ylidene malononitrile, polypyridyl donors, SC-XRD
1422-8599
Podda, Enrico
14a14e34-7d30-440d-83d6-004332a23a0e
Arca, Massimiliano
f90b59f6-4dfb-471d-912e-3515e6507165
Pintus, Anna
d2ae260a-d159-48a7-b000-539e8c19c68e
Meloni, Francesca
5bf79e2e-04de-4f63-a699-f6ad864f4ec4
Lippolis, Vito
d9833a14-4aab-4827-a2ba-be818871dcf5
Ferino, Giulio
5b21ac2b-c3f6-4988-b562-455abe07fa46
Orton, James B.
4e2a471f-9e11-4cb4-abb6-d0398047939f
Coles, Simon J.
3116f58b-c30c-48cf-bdd5-397d1c1fecf8
Aragoni, Maria Carla
e2a7410a-65e0-4550-afba-0d3282d34190
Podda, Enrico
14a14e34-7d30-440d-83d6-004332a23a0e
Arca, Massimiliano
f90b59f6-4dfb-471d-912e-3515e6507165
Pintus, Anna
d2ae260a-d159-48a7-b000-539e8c19c68e
Meloni, Francesca
5bf79e2e-04de-4f63-a699-f6ad864f4ec4
Lippolis, Vito
d9833a14-4aab-4827-a2ba-be818871dcf5
Ferino, Giulio
5b21ac2b-c3f6-4988-b562-455abe07fa46
Orton, James B.
4e2a471f-9e11-4cb4-abb6-d0398047939f
Coles, Simon J.
3116f58b-c30c-48cf-bdd5-397d1c1fecf8
Aragoni, Maria Carla
e2a7410a-65e0-4550-afba-0d3282d34190

Podda, Enrico, Arca, Massimiliano, Pintus, Anna, Meloni, Francesca, Lippolis, Vito, Ferino, Giulio, Orton, James B., Coles, Simon J. and Aragoni, Maria Carla (2023) 2-(2,7-Bis(pyridin-3-ylethynyl)fluoren-9-ylidene)malononitrile. Molbank, 2023 (2), [M1619]. (doi:10.3390/M1619).

Record type: Article

Abstract

The 2-(2,7-bis(pyridin-3-ylethynyl)fluoren-9-ylidene)malononitrile (1) was synthesized by reaction of 2,7-bis(pyridin-3-ylethynyl)fluoren-9-one with malononitrile in DMSO solution. The structural characterization of 1 by SC-XRD analysis was accompanied by elemental analysis, FT-IR, NMR, and MS measurements.

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molbank-2023-M1619-v2 - Version of Record
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Accepted/In Press date: 7 April 2023
Published date: June 2023
Additional Information: Funding Information: The authors acknowledge Fondazione di Sardegna (FdS Progetti Biennali di Ateneo, annualità 2018) for financial support and the EPSRC (Engineering and Physical Science Research Council) for the continued support of the UK’s National Crystallography Service (NCS), based at the University of Southampton. Publisher Copyright: © 2023 by the authors.
Keywords: fluoren-9-ylidene malononitrile, polypyridyl donors, SC-XRD

Identifiers

Local EPrints ID: 480957
URI: http://eprints.soton.ac.uk/id/eprint/480957
DOI: doi:10.3390/M1619
ISSN: 1422-8599
PURE UUID: 18a7f189-87c8-4b0d-b06a-201e9f19b898
ORCID for Simon J. Coles: ORCID iD orcid.org/0000-0001-8414-9272

Catalogue record

Date deposited: 11 Aug 2023 17:07
Last modified: 18 Mar 2024 02:50

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Contributors

Author: Enrico Podda
Author: Massimiliano Arca
Author: Anna Pintus
Author: Francesca Meloni
Author: Vito Lippolis
Author: Giulio Ferino
Author: James B. Orton
Author: Simon J. Coles ORCID iD
Author: Maria Carla Aragoni

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