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A comparative study between AZ31 and Mg-Gd alloys after high-pressure torsion

A comparative study between AZ31 and Mg-Gd alloys after high-pressure torsion
A comparative study between AZ31 and Mg-Gd alloys after high-pressure torsion

The evolution of microstructure, texture, and mechanical properties of AZ31 (Mg-3Al-1Zn, wt.%) and Mg-0.6Gd (wt.%) alloys was investigated and compared after high-pressure torsion at room temperature through the equivalent strain range of ε eq = 0.6 − 287.5. The results demonstrated that the grain refinement behavior is different for these two alloys. For the AZ31 alloy, dynamic recrystallization (DRX) was restricted leading to a gradual and continuous formation of ultrafine grains with a mean grain size of ~ 0.3 µm through the entire strain range and the development of deviated B, C 1, and C 2 texture fibers. For the Mg-0.6Gd alloy, the DRX was very fast and a rapid ultrafine grain microstructure with a mean grain size of ~ 0.7 µm was developed at a strain range of ε eq = 0.6 − 5.7 and this remained stable with a relatively stable B-fiber over the strain range ε eq = 5.7 − 287.5. The evolution of microhardness in the AZ31 alloy indicated a strain hardening without recovery while that of the Mg-0.6Gd alloy showed a strain hardening with recovery. The differences between the AZ31 and Mg-0.6Gd alloys are discussed based on a comprehensive characterization of twinning, dislocation density, the initial microstructure and the presence of second phases.

dynamic recrystallization, high-pressure torsion, magnesium, microstructure, rare-earth, texture
1059-9495
Ould Mohamed, Ouarda
6f592835-5ba6-4160-a9a7-0e395e0521f5
Bazarnik, Piotr
7612d50d-0cfc-43b1-a48f-f5062caacc1e
Huang, Yi
9f4df815-51c1-4ee8-ad63-a92bf997103e
Azzeddine, Hiba
f32633f8-2f8a-433e-9180-ada2b8704eae
Baudin, Thierry
933b263a-4a22-4c65-9599-16b27346e946
Brisset, François
c93ca177-5b75-400d-a9fb-85a567cebec6
Langdon, Terence G.
86e69b4f-e16d-4830-bf8a-5a9c11f0de86
Ould Mohamed, Ouarda
6f592835-5ba6-4160-a9a7-0e395e0521f5
Bazarnik, Piotr
7612d50d-0cfc-43b1-a48f-f5062caacc1e
Huang, Yi
9f4df815-51c1-4ee8-ad63-a92bf997103e
Azzeddine, Hiba
f32633f8-2f8a-433e-9180-ada2b8704eae
Baudin, Thierry
933b263a-4a22-4c65-9599-16b27346e946
Brisset, François
c93ca177-5b75-400d-a9fb-85a567cebec6
Langdon, Terence G.
86e69b4f-e16d-4830-bf8a-5a9c11f0de86

Ould Mohamed, Ouarda, Bazarnik, Piotr, Huang, Yi, Azzeddine, Hiba, Baudin, Thierry, Brisset, François and Langdon, Terence G. (2023) A comparative study between AZ31 and Mg-Gd alloys after high-pressure torsion. Journal of Materials Engineering and Performance. (doi:10.1007/s11665-023-08856-8).

Record type: Article

Abstract

The evolution of microstructure, texture, and mechanical properties of AZ31 (Mg-3Al-1Zn, wt.%) and Mg-0.6Gd (wt.%) alloys was investigated and compared after high-pressure torsion at room temperature through the equivalent strain range of ε eq = 0.6 − 287.5. The results demonstrated that the grain refinement behavior is different for these two alloys. For the AZ31 alloy, dynamic recrystallization (DRX) was restricted leading to a gradual and continuous formation of ultrafine grains with a mean grain size of ~ 0.3 µm through the entire strain range and the development of deviated B, C 1, and C 2 texture fibers. For the Mg-0.6Gd alloy, the DRX was very fast and a rapid ultrafine grain microstructure with a mean grain size of ~ 0.7 µm was developed at a strain range of ε eq = 0.6 − 5.7 and this remained stable with a relatively stable B-fiber over the strain range ε eq = 5.7 − 287.5. The evolution of microhardness in the AZ31 alloy indicated a strain hardening without recovery while that of the Mg-0.6Gd alloy showed a strain hardening with recovery. The differences between the AZ31 and Mg-0.6Gd alloys are discussed based on a comprehensive characterization of twinning, dislocation density, the initial microstructure and the presence of second phases.

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Accepted/In Press date: 5 October 2023
e-pub ahead of print date: 19 October 2023
Additional Information: Funding Information: Dr-Ing. N. Hort and Dr. D. Letzig (MagIC, Germany) and Dr-Ing. Talal Al-Samman (RWTH-Aachen University, Germany) are gratefully acknowledged for providing the AZ31 and Mg-0.6Gd alloys, respectively. Two of the authors were supported by the European Research Council under Grant Agreement No. 267464-SPDMETALS (YH and TGL). Publisher Copyright: © 2023, ASM International.
Keywords: dynamic recrystallization, high-pressure torsion, magnesium, microstructure, rare-earth, texture

Identifiers

Local EPrints ID: 483112
URI: http://eprints.soton.ac.uk/id/eprint/483112
ISSN: 1059-9495
PURE UUID: 208b6dae-5634-4d5d-a149-9700387785f4
ORCID for Yi Huang: ORCID iD orcid.org/0000-0001-9259-8123
ORCID for Terence G. Langdon: ORCID iD orcid.org/0000-0003-3541-9250

Catalogue record

Date deposited: 23 Oct 2023 17:04
Last modified: 18 Mar 2024 03:19

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Contributors

Author: Ouarda Ould Mohamed
Author: Piotr Bazarnik
Author: Yi Huang ORCID iD
Author: Hiba Azzeddine
Author: Thierry Baudin
Author: François Brisset

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