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Significance of adiabatic heating on phase transformation in titanium-based alloys during severe plastic deformation

Significance of adiabatic heating on phase transformation in titanium-based alloys during severe plastic deformation
Significance of adiabatic heating on phase transformation in titanium-based alloys during severe plastic deformation
Experiments were conducted on Ti-based alloys including a commercially pure titanium (α phase), Ti-6Al-4 V (α + β phase) and TiNi (B19’-martensitic phase) alloys in order to investigate the phase transformation during high-pressure torsion (HPT) at room temperature. An allotropic α to ω phase transformation in the commercially pure titanium occurred during HPT processing but increasing the rotation speed led to a decrease in the volume fraction of the ω-phase. This procedure facilitates the loss of the β phase in the Ti-6Al-4 V alloy and promotes a B19’ to B2 (austenite) phase transformation in the TiNi alloy. The results show that the bulk temperature increment in the processed specimens was not sufficiently high to affect phase transformations. However, the calculations by assuming adiabatic conditions revealed that the local temperature increment is responsible to encourage or suppress the phase transformation in the Ti-based alloys. This fundamental understanding of phase transformations during severe plastic deformation is useful for conducting microstructure engineering of Ti-based alloys by tailoring the microstructures containing different phases and thereby producing different mechanical and functional behaviors.
Adiabatic heating, High-pressure torsion, Microstructure engineering, Phase transformation, Severe plastic deformation, Ti-based alloys
1044-5803
Shahmir, Hamed
6914819d-f654-4928-a445-9ac0d3abedcf
Nili-Ahmadabadi, Mahmoud
74c5b0be-a73e-40fe-bc6e-8450bc0eeaf7
Kim, Hyoung Seop
762e00dc-3fa4-49ec-85d5-0f5bab01399b
Langdon, Terence G.
86e69b4f-e16d-4830-bf8a-5a9c11f0de86
Shahmir, Hamed
6914819d-f654-4928-a445-9ac0d3abedcf
Nili-Ahmadabadi, Mahmoud
74c5b0be-a73e-40fe-bc6e-8450bc0eeaf7
Kim, Hyoung Seop
762e00dc-3fa4-49ec-85d5-0f5bab01399b
Langdon, Terence G.
86e69b4f-e16d-4830-bf8a-5a9c11f0de86

Shahmir, Hamed, Nili-Ahmadabadi, Mahmoud, Kim, Hyoung Seop and Langdon, Terence G. (2023) Significance of adiabatic heating on phase transformation in titanium-based alloys during severe plastic deformation. Materials Characterization, 203, [113091]. (doi:10.1016/j.matchar.2023.113091).

Record type: Article

Abstract

Experiments were conducted on Ti-based alloys including a commercially pure titanium (α phase), Ti-6Al-4 V (α + β phase) and TiNi (B19’-martensitic phase) alloys in order to investigate the phase transformation during high-pressure torsion (HPT) at room temperature. An allotropic α to ω phase transformation in the commercially pure titanium occurred during HPT processing but increasing the rotation speed led to a decrease in the volume fraction of the ω-phase. This procedure facilitates the loss of the β phase in the Ti-6Al-4 V alloy and promotes a B19’ to B2 (austenite) phase transformation in the TiNi alloy. The results show that the bulk temperature increment in the processed specimens was not sufficiently high to affect phase transformations. However, the calculations by assuming adiabatic conditions revealed that the local temperature increment is responsible to encourage or suppress the phase transformation in the Ti-based alloys. This fundamental understanding of phase transformations during severe plastic deformation is useful for conducting microstructure engineering of Ti-based alloys by tailoring the microstructures containing different phases and thereby producing different mechanical and functional behaviors.

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More information

Accepted/In Press date: 10 June 2023
e-pub ahead of print date: 12 June 2023
Published date: 23 June 2023
Additional Information: Funding Information: This work was supported by the National Elites Foundation of the Islamic Republic of Iran and in part by the European Research Council under Grant Agreement No. 267464-SPDMETALS (TGL). In addition, the work was supported by the National Research Foundation of Korea (NRF) with a grant funded by the Korea government (MSIP) (No. 2014R1A2A1A10051322 ). The authors thank Southampton Nanofabrication Center for assistance in TEM sample preparation using FIB.
Keywords: Adiabatic heating, High-pressure torsion, Microstructure engineering, Phase transformation, Severe plastic deformation, Ti-based alloys

Identifiers

Local EPrints ID: 483430
URI: http://eprints.soton.ac.uk/id/eprint/483430
ISSN: 1044-5803
PURE UUID: 87609b3f-26fc-4c01-bff8-22b4df6f3f64
ORCID for Terence G. Langdon: ORCID iD orcid.org/0000-0003-3541-9250

Catalogue record

Date deposited: 30 Oct 2023 18:03
Last modified: 06 Jun 2024 01:40

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Contributors

Author: Hamed Shahmir
Author: Mahmoud Nili-Ahmadabadi
Author: Hyoung Seop Kim

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