N,N′-Dibutyloxamide
N,N′-Dibutyloxamide
N,N′-dibutyloxamide (1) was prepared by reacting diethyloxalate with n-butylamine in ethyl alcohol and characterized by microanalytical techniques, FT-IR, and NMR spectroscopy. Crystals suitable for single crystal X-ray diffraction (SC-XRD) were obtained from an acetonitrile solution of 1, and the structural characterization showed the presence of intermolecular hydrogen bonding interactions.
N,N′-dialkyloxamides, oxalamides, oxalic acid derivatives, oxamide ligands, XRD
Podda, Enrico
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Dodd, Eleanor
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Arca, Massimiliano
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Aragoni, M. Carla
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Lippolis, Vito
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Coles, Simon J.
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Pintus, Anna
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Podda, Enrico
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Dodd, Eleanor
c03a883b-724d-4717-90d3-ec7307d73ac0
Arca, Massimiliano
f90b59f6-4dfb-471d-912e-3515e6507165
Aragoni, M. Carla
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Lippolis, Vito
d9833a14-4aab-4827-a2ba-be818871dcf5
Coles, Simon J.
3116f58b-c30c-48cf-bdd5-397d1c1fecf8
Pintus, Anna
d2ae260a-d159-48a7-b000-539e8c19c68e
Podda, Enrico, Dodd, Eleanor, Arca, Massimiliano, Aragoni, M. Carla, Lippolis, Vito, Coles, Simon J. and Pintus, Anna
(2023)
N,N′-Dibutyloxamide.
Molbank, 2023 (3), [M1677].
(doi:10.3390/M1677).
Abstract
N,N′-dibutyloxamide (1) was prepared by reacting diethyloxalate with n-butylamine in ethyl alcohol and characterized by microanalytical techniques, FT-IR, and NMR spectroscopy. Crystals suitable for single crystal X-ray diffraction (SC-XRD) were obtained from an acetonitrile solution of 1, and the structural characterization showed the presence of intermolecular hydrogen bonding interactions.
Text
molbank-2023-M1677
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Accepted/In Press date: 27 June 2023
e-pub ahead of print date: 29 June 2023
Additional Information:
Funding Information:
The authors acknowledge Fondazione di Sardegna (FdS Progetti Biennali di Ateneo, annualità 2018) for financial support.
Keywords:
N,N′-dialkyloxamides, oxalamides, oxalic acid derivatives, oxamide ligands, XRD
Identifiers
Local EPrints ID: 483726
URI: http://eprints.soton.ac.uk/id/eprint/483726
ISSN: 1422-8599
PURE UUID: d4b10cbd-ef51-4283-b6fb-d46bb864e742
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Date deposited: 03 Nov 2023 18:00
Last modified: 18 Mar 2024 02:50
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Contributors
Author:
Enrico Podda
Author:
Eleanor Dodd
Author:
Massimiliano Arca
Author:
M. Carla Aragoni
Author:
Vito Lippolis
Author:
Anna Pintus
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