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Characterisation of white etching structures formed in annealed AISI 52100 through High Pressure Torsion (HPT)

Characterisation of white etching structures formed in annealed AISI 52100 through High Pressure Torsion (HPT)
Characterisation of white etching structures formed in annealed AISI 52100 through High Pressure Torsion (HPT)
White Etching Structures (WES) similar to white etching areas observed in rolling bearings have been obtained after conducting High Pressure Torsion tests (HPT) on annealed AISI 52100-disc samples. This paper presents results from the detailed analysis of these WES using Electron Backscatter Diffraction (EBSD) and Energy-dispersive X-ray Spectroscopy (EDS). EBSD analysis suggests WES consisted of a nano structured material, whilst EDS analysis revealed redistributions of carbon and chromium contents inside WES compared to the surrounding matrix. It appears the plastic deformation induced by HPT has led to degradation and dissolution of the carbides present in the as annealed microstructure and the formation of a nanocrystalline structure. No evidence of recrystallization process was registered either inside WES or in their vicinities.
AISI 52100, Carbide dissolution, High-Pressure Torsion, White Etching Areas
0301-679X
Wilches Pena, Luis Vicente
Wang, Ling
c50767b1-7474-4094-9b06-4fe64e9fe362
Mellor, B.G.
2b13b80f-880b-49ac-82fe-827a15dde2fe
Schwedt, Alexander
d3c68d66-55d0-43a4-8cbf-c75b5aa27df4
Mayer, J.
2c4ab1f9-1d97-4339-bb92-c0e6a0b67209
Holweger, Walter
8160e635-5bb4-438f-89e7-3beb7abdc56a
Wilches Pena, Luis Vicente
Wang, Ling
c50767b1-7474-4094-9b06-4fe64e9fe362
Mellor, B.G.
2b13b80f-880b-49ac-82fe-827a15dde2fe
Schwedt, Alexander
d3c68d66-55d0-43a4-8cbf-c75b5aa27df4
Mayer, J.
2c4ab1f9-1d97-4339-bb92-c0e6a0b67209
Holweger, Walter
8160e635-5bb4-438f-89e7-3beb7abdc56a

Wilches Pena, Luis Vicente, Wang, Ling, Mellor, B.G., Schwedt, Alexander, Mayer, J. and Holweger, Walter (2023) Characterisation of white etching structures formed in annealed AISI 52100 through High Pressure Torsion (HPT). Tribology International, 184, [108432]. (doi:10.1016/j.triboint.2023.108432).

Record type: Article

Abstract

White Etching Structures (WES) similar to white etching areas observed in rolling bearings have been obtained after conducting High Pressure Torsion tests (HPT) on annealed AISI 52100-disc samples. This paper presents results from the detailed analysis of these WES using Electron Backscatter Diffraction (EBSD) and Energy-dispersive X-ray Spectroscopy (EDS). EBSD analysis suggests WES consisted of a nano structured material, whilst EDS analysis revealed redistributions of carbon and chromium contents inside WES compared to the surrounding matrix. It appears the plastic deformation induced by HPT has led to degradation and dissolution of the carbides present in the as annealed microstructure and the formation of a nanocrystalline structure. No evidence of recrystallization process was registered either inside WES or in their vicinities.

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Accepted/In Press date: 18 March 2023
e-pub ahead of print date: 21 March 2023
Published date: June 2023
Additional Information: Funding Information: This research has been co-funded by the National Centre of Advanced Tribology at Southampton – nCATS at the University of Southampton (UK), the Universidad EIA (Envigado, Antioquia Colombia), the Colombian Administrative Department of Science, Technology and Innovation – Colciencias (Colombia), and the Agency for Higher Education - Sapiencia, Enlazamundos Program (Colombia). Publisher Copyright: © 2023
Keywords: AISI 52100, Carbide dissolution, High-Pressure Torsion, White Etching Areas

Identifiers

Local EPrints ID: 484628
URI: http://eprints.soton.ac.uk/id/eprint/484628
ISSN: 0301-679X
PURE UUID: f9c51c42-4162-4a27-8ed9-cf75eeaa1051
ORCID for Ling Wang: ORCID iD orcid.org/0000-0002-2894-6784

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Date deposited: 17 Nov 2023 18:09
Last modified: 17 Mar 2024 02:55

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Contributors

Author: Luis Vicente Wilches Pena
Author: Ling Wang ORCID iD
Author: B.G. Mellor
Author: Alexander Schwedt
Author: J. Mayer
Author: Walter Holweger

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