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Correlation between microstructure, magnetic properties and mechanical behavior of the permimphy alloy after high-pressure torsion

Correlation between microstructure, magnetic properties and mechanical behavior of the permimphy alloy after high-pressure torsion
Correlation between microstructure, magnetic properties and mechanical behavior of the permimphy alloy after high-pressure torsion
This study investigates the correlation between coercivity (Hc), grain size (d), and
dislocation density in the Permimphy alloy (Fe-80%Ni-6%Mo). The samples used in this study were subjected to varying levels of applied strain through processing by high-pressure torsion (HPT). The microstructure and the magnetic coercivity were analyzed using a scanning electron microscope (SEM), Electron Backscatter Diffraction (EBSD) and Vibrating Sample Magnetometry (VSM). The grain size of the samples varied from 30 µm to 190 nm. This study demonstrated a strong correlation between Hc and microhardness when d > 3 µm. The results show that the coercivity of the Permimphy alloy follows an inverse V-shape with respect to grain size. The coercivity of the samples decreased despite increasing the dislocation density and the hardness when d < 3 µm. This phenomenon is attributed to the ferromagnetic exchange interaction across multiple grains and leads to the alignment of magnetic moments.
permimphy, high-pressure torsion, microstructure, hardness, coercivity, dislocations
0022-2461
Dabou, Oussama
9658641e-4b95-49b3-860b-0623c6df03b4
Baudin, Thierry
933b263a-4a22-4c65-9599-16b27346e946
Brisset, François
c93ca177-5b75-400d-a9fb-85a567cebec6
Waeckerlé, Thierry
337d49c6-7a38-475f-b942-45a52a03b6bb
Ateba Betanda, Yanick
b3b55bd0-10ee-43d1-b859-f539f18d00cb
Huang, Yi
9f4df815-51c1-4ee8-ad63-a92bf997103e
Helbert, Anne-Laure
01ac4ac4-73d6-4649-9bf5-4be30f1e6df2
Bradai, Djamel
554ec639-52df-4169-8044-53485b61c829
Langdon, Terence G.
86e69b4f-e16d-4830-bf8a-5a9c11f0de86
Dabou, Oussama
9658641e-4b95-49b3-860b-0623c6df03b4
Baudin, Thierry
933b263a-4a22-4c65-9599-16b27346e946
Brisset, François
c93ca177-5b75-400d-a9fb-85a567cebec6
Waeckerlé, Thierry
337d49c6-7a38-475f-b942-45a52a03b6bb
Ateba Betanda, Yanick
b3b55bd0-10ee-43d1-b859-f539f18d00cb
Huang, Yi
9f4df815-51c1-4ee8-ad63-a92bf997103e
Helbert, Anne-Laure
01ac4ac4-73d6-4649-9bf5-4be30f1e6df2
Bradai, Djamel
554ec639-52df-4169-8044-53485b61c829
Langdon, Terence G.
86e69b4f-e16d-4830-bf8a-5a9c11f0de86

Dabou, Oussama, Baudin, Thierry, Brisset, François, Waeckerlé, Thierry, Ateba Betanda, Yanick, Huang, Yi, Helbert, Anne-Laure, Bradai, Djamel and Langdon, Terence G. (2024) Correlation between microstructure, magnetic properties and mechanical behavior of the permimphy alloy after high-pressure torsion. Journal of Materials Science. (In Press)

Record type: Article

Abstract

This study investigates the correlation between coercivity (Hc), grain size (d), and
dislocation density in the Permimphy alloy (Fe-80%Ni-6%Mo). The samples used in this study were subjected to varying levels of applied strain through processing by high-pressure torsion (HPT). The microstructure and the magnetic coercivity were analyzed using a scanning electron microscope (SEM), Electron Backscatter Diffraction (EBSD) and Vibrating Sample Magnetometry (VSM). The grain size of the samples varied from 30 µm to 190 nm. This study demonstrated a strong correlation between Hc and microhardness when d > 3 µm. The results show that the coercivity of the Permimphy alloy follows an inverse V-shape with respect to grain size. The coercivity of the samples decreased despite increasing the dislocation density and the hardness when d < 3 µm. This phenomenon is attributed to the ferromagnetic exchange interaction across multiple grains and leads to the alignment of magnetic moments.

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Dabou et al - Accepted Manuscript
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Accepted/In Press date: 7 February 2024
Keywords: permimphy, high-pressure torsion, microstructure, hardness, coercivity, dislocations

Identifiers

Local EPrints ID: 486981
URI: http://eprints.soton.ac.uk/id/eprint/486981
ISSN: 0022-2461
PURE UUID: f04cd25a-ec1c-4a08-a1ee-2456cb01adca
ORCID for Yi Huang: ORCID iD orcid.org/0000-0001-9259-8123
ORCID for Terence G. Langdon: ORCID iD orcid.org/0000-0003-3541-9250

Catalogue record

Date deposited: 09 Feb 2024 17:32
Last modified: 18 Mar 2024 03:19

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Contributors

Author: Oussama Dabou
Author: Thierry Baudin
Author: François Brisset
Author: Thierry Waeckerlé
Author: Yanick Ateba Betanda
Author: Yi Huang ORCID iD
Author: Anne-Laure Helbert
Author: Djamel Bradai

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