N,N′-Dipropyloxamide
N,N′-Dipropyloxamide
N,N′-Dipropyloxamide (1) was synthesised by the reaction between diethyloxalate and n-propylamine in ethanol. Compound 1 was fully characterised by both microanalytical (elemental analysis, melting point determination) and spectroscopic means (FT-IR and NMR spectroscopy). Crystals suitable for single crystal X-ray diffraction were isolated by the slow evaporation of a methyl alcohol solution of the compound. The resulting crystal structure shows the prominent role exerted by intermolecular hydrogen bonds in the crystal packing.
hydrogen bond, N,N′-dialkyloxamides, oxalamides, oxalic acid derivatives, XRD
Podda, Enrico
14a14e34-7d30-440d-83d6-004332a23a0e
Dodd, Eleanor
c03a883b-724d-4717-90d3-ec7307d73ac0
Arca, Massimiliano
f90b59f6-4dfb-471d-912e-3515e6507165
Aragoni, M. Carla
3e73ed7a-2cf7-4f5e-9359-61d6e34a6cd5
Lippolis, Vito
d9833a14-4aab-4827-a2ba-be818871dcf5
Coles, Simon J.
3116f58b-c30c-48cf-bdd5-397d1c1fecf8
Pintus, Anna
d2ae260a-d159-48a7-b000-539e8c19c68e
22 December 2023
Podda, Enrico
14a14e34-7d30-440d-83d6-004332a23a0e
Dodd, Eleanor
c03a883b-724d-4717-90d3-ec7307d73ac0
Arca, Massimiliano
f90b59f6-4dfb-471d-912e-3515e6507165
Aragoni, M. Carla
3e73ed7a-2cf7-4f5e-9359-61d6e34a6cd5
Lippolis, Vito
d9833a14-4aab-4827-a2ba-be818871dcf5
Coles, Simon J.
3116f58b-c30c-48cf-bdd5-397d1c1fecf8
Pintus, Anna
d2ae260a-d159-48a7-b000-539e8c19c68e
Podda, Enrico, Dodd, Eleanor, Arca, Massimiliano, Aragoni, M. Carla, Lippolis, Vito, Coles, Simon J. and Pintus, Anna
(2023)
N,N′-Dipropyloxamide.
Molbank, 2024 (1), [M1753].
(doi:10.3390/M1753).
Abstract
N,N′-Dipropyloxamide (1) was synthesised by the reaction between diethyloxalate and n-propylamine in ethanol. Compound 1 was fully characterised by both microanalytical (elemental analysis, melting point determination) and spectroscopic means (FT-IR and NMR spectroscopy). Crystals suitable for single crystal X-ray diffraction were isolated by the slow evaporation of a methyl alcohol solution of the compound. The resulting crystal structure shows the prominent role exerted by intermolecular hydrogen bonds in the crystal packing.
Text
molbank-2024-M1753
- Version of Record
More information
Accepted/In Press date: 18 December 2023
Published date: 22 December 2023
Keywords:
hydrogen bond, N,N′-dialkyloxamides, oxalamides, oxalic acid derivatives, XRD
Identifiers
Local EPrints ID: 489099
URI: http://eprints.soton.ac.uk/id/eprint/489099
ISSN: 1422-8599
PURE UUID: 47a7a2f8-b165-4269-84cd-8cb56fa4521f
Catalogue record
Date deposited: 15 Apr 2024 16:31
Last modified: 16 Apr 2024 01:36
Export record
Altmetrics
Contributors
Author:
Enrico Podda
Author:
Eleanor Dodd
Author:
Massimiliano Arca
Author:
M. Carla Aragoni
Author:
Vito Lippolis
Author:
Anna Pintus
Download statistics
Downloads from ePrints over the past year. Other digital versions may also be available to download e.g. from the publisher's website.
View more statistics
